Two-Dimensional NMR Methods for Establishing Molecular Connectivity
A Chemist's Guide to Experiment Selection, Performance, and Interpretation

G. E. Martin (Author), A. S. Zektzer (Author)

9780471187073, Wiley

Hardback, published 21 October 1988

528 pages
24.4 x 16.2 x 3.3 cm, 0.903 kg

This guide to two-dimensional NMR spectroscopy helps the novice who want e the technique, but needs a path through the bewildering array of metho acronyms and the mathematical rigor found in most books.
The authors provide a clear explanation of experiment performance, param lection, data processing and presentation as well as a description of wh rmation is provided by each experiment and how it is extracted and inter They group presentations of two-dimensional NMR experiments according t zation, e.g. COSY, LRCOSY, ZQCOSY, DQCOSY ... for establishing proton-pr nnectivities.
The book also presents spectra of the same model compound using various ues to enable the reader to make direct comparisons and facilitate his e nt selection. Examples of the concerted utilization of various two-dimen NMR experiments to solve complex structural problems are also given.

Introduction and Practical Considerations of Two-Dimensional NMR Spectroscopy.

Heteronuclear Chemical shift Correlation.

Relayed Coherence Transfer and Related 2D-NMR Experiments.

13_C-13_C Double Coherence 2D-NMR. The Inadequate Experiments.

Applications Problems.

Solutions to Problems.

Index.

Subject Areas: Chemistry [PN]