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Pyrolysis - GC/MS Data Book of Synthetic Polymers
Pyrograms, Thermograms and MS of Pyrolyzates
Shin Tsuge (Author), Hajima Ohtani (Author), Chuichi Watanabe (Author)
9780444538925, Elsevier Science
Hardback, published 6 September 2011
420 pages
23.4 x 19 x 2.7 cm, 0.86 kg
In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers.
1. Preface2. Introduction3. Pyrograms and Thermograms of 163 High Polymers, and MS Data of the Major Pyrolyzates4. Pyrograms for 33 Condensation Polymers and MS Data of the Major Pyrolyzates Obtained in the Presence of Organic Alkaline5. Appendix Monographs and Reviews for Pyrolysis-GC of Polymers
Subject Areas: Polymer chemistry [PNNP], Spectrum analysis, spectrochemistry, mass spectrometry [PNFS], Analytical chemistry [PNF]