Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers

John S. Harwood (Author), Huaping Mo (Author)

9780128006894, Elsevier Science

Paperback, published 27 October 2015

136 pages, 40 illustrations
22.9 x 15.1 x 1 cm, 0.25 kg

Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge’s High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009).

Introduction1. Basics and Spectrometer Performance Checks2. Multiple Irradiation and Multiple Pulse Experiments3. Polarization Transfer and Its Applications4. Homonuclear Correlation Experiments5. PFG (Pulsed Field Gradient) Experiments6. Introduction to NMR of Biomolecules in H₂O7. Selective Experiments Using Shaped Pulses8. Diffusion Measurements and DOSY (Diffusion Ordered SpectroscopY)

Subject Areas: Spectrum analysis, spectrochemistry, mass spectrometry [PNFS], Electricity, electromagnetism & magnetism [PHK], Scientific equipment, experiments & techniques [PDN]