Freshly Printed - allow 7 days lead
Couldn't load pickup availability
Organic Syntheses, Volume 96
John L Wood (Author)
9781119707769, Wiley
Hardback, published 20 May 2020
656 pages
23.4 x 15.8 x 3 cm, 0.885 kg
The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.
Discussion Addendum for: 4-Nonylbenzoic Acid 1 Late-Stage Deoxyfluorination of Phenols with PhenoFluorMix 16 Nickel-Catalyzed Cross-Coupling of 2-Methoxynaphthalene with Methyl 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzoate 36 Discussion Addendum for: Lithium Amides as Homochiral Ammonia Equivalents for Conjugate Additions to α,β-Unsaturated Esters: Asymmetric Synthesis of (S)-β-Leucine 53 Synthesis of 2,3-Diaryl-2H-azirines via Cs2CO3-Mediated Cyclization of Ketoxime Acetates 66 Discussion Addendum for: The Direct Acyl-Alkylation of Arynes. Preparation of Methyl 2- (2-acetylphenyl)acetate 80 Discussion Addendum for: Convenient Preparation of 3-Ethoxycarbonyl Benzofurans from Salicylaldehydes and Ethyl Diazoacetate 98 Discussion Addendum for: Phosphine-Catalyzed [4 + 2] Annulation: Synthesis of Ethyl 6-Phenyl-1-tosyl-1,2,5,6-tetrahydropyridine-3-carboxylate 110 Discussion Addendum for: Protection of Alcohols using 2-Benzyloxy-1-methylpyridinium Trifluoromethanesulfonate: Methyl (R)-(-)-3-Benzyloxy-2-methyl Propanoate 124 Synthesis of 4-Methylbenzoate(2′,4′,6′-trimethoxy-phenyl)iodonium Tosylate 137 Gold-Catalyzed Oxidative Coupling of Arenes and Arylsilanes 150 Discussion Addendum for: Preparation of Enantioenriched Homoallylic Primary Amines 179 Discussion Addendum for: Synthesis of Ynamides by Copper-Mediated Coupling of 1,1-Dibromo-1-alkenes with Nitrogen Nucleophiles. Preparation of 4-Methyl-N-(2-phenylethynyl)-N-(phenylmethyl)benzenesulfonamide 195 Discussion Addendum for: Phosphine-Catalyzed [3 + 2] Annulation: Synthesis of Ethyl 5-(tert-Butyl)-2-phenyl-1-tosyl-3-pyrroline-3-carboxylate 214 Discussion Addendum for: Synthesis of Highly Enantiomerically Enriched Amines by Asymmetric Transfer Hydrogenation of N-(tert-Butylsulfinyl) Imines 232 Synthesis of Chiral Diamine Ligands for Nickel-catalyzed Asymmetric Cross-couplings of Alkylchloroboronate Esters with Alkylzincs: 1R,2R)-N,N’-Dimethyl-1,2-bis(2-methylphenyl)-1,2-diaminoethane 245 Preparation of 5-(Triisopropylalkynyl) dibenzo[b,d] thiophenium triflate 258 Three-Step Synthesis of 2-(Diiodomethyl)-4,4,5,5-tetramethyl- 1,3,2-dioxaborolane from Dichloromethane 277 Discussion Addendum for: Allylic Oxidation Catalyzed by Dirhodium(II) Tetrakis[ε-caprolactamate] of tert-Butyldimethylsilylprotected trans-Dehydroandrosterone 300 Preparation of (R)-3-(3,5-Bistrifluoromethylphenyl)-1,1’-bi-2-naphthol 312 Catalytic Enantioselective Addition of an In-Situ Prepared Aryltitanium Reagent to p-Chloroacetophenone: (R)-(+)-1-(4-Chlorophenyl)-1-m-tolylethanol 333 Stereoselective Synthesis of (R)-((R)-1-Phenyl-2,2,2-trichloroethyl)-2-(2-bromophenyl)aziridine-1-carboxylate 351 Discussion Addendum for: Preparation of (R,R)-1,2:4,5-Diepoxypentane 361 (R)-N,N’-Dimethyl-1,1’-binaphthyldiamine 382 Preparation of a Diisopropylselenophosphoramide Catalyst and its Use in Enantioselective Sulfenoetherification 400 anti-1,2,2,3,4,4-Hexamethylphosphetane 1-Oxide 418 Facile Reduction of Amides Using Nickel Catalysis: Reduction of 12-Aminododecanolactam 436 Preparation of 2,4,5,6-Tetra(9H-carbazol-9-yl)isophthalonitrile 455 Discussion Addendum for: Fluorobis(phenylsulfonyl)methane (FBSM) 474 Synthesis of 5-Hydroxy-4-methoxy-2-methylpyrylium Trifluoromethanesulfonate from Kojic Acid 494 Iridium-Catalyzed Reductive Coupling of Grignard Reagents and Tertiary Amides 511 Synthesis of Chiral Tetramic Acids: Preparation of (S)-5-Benzylpyrrolidine-2,4-dione from L-Phenylalanine Methyl Ester Hydrochloride 528 Synthesis of 8-Hydroxygeraniol 586
Alois Fürstner
Junting Chen and Tobias Ritter
Yuki Kawashima, Takayuki Furukawa, Naoto Chatani and Mamoru Tobisu
Stephen G. Davies, Ai M. Fletcher, Paul M. Roberts, and James E. Thomson
Mi-Na Zhao and Zheng-Hui Guan
Austin C. Wright and Brian M. Stoltz
Mizzanoor Rahaman and M. Mahmun Hossain
Aslam C. Shaikh and Ohyun Kwon
Harvey F. Fulo, Philip A. Albiniak, and Gregory B. Dudley
Thomas L. Seidl, Aaron Moment, Charles Orella, Thomas Vickery, and David R. Stuart
Chris Nottingham, Verity Barber, and Guy C. Lloyd-Jones
Miguel Yus
Cédric Theunissen, Pierre Thilmany, Mounsef Lahboubi, Nicolas Blanchard, and Gwilherm Evano
Aslam C. Shaikh and Ohuyn Kwon
Miguel Yus
Yusuke Masuda and Gregory C. Fu
Bernd Waldecker, Kevin Kafuta, and Manuel Alcarazo
Morgane Sayes, Guillaume Benoit, and André B. Charette
Yong-Liang Su, Luca De Angelis and Michael P. Doyle
Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada
Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada
Hélène Lebel and Henri Piras
Nicholas Sizemore and Scott D. Rychnovsky
Scott E. Denmark and Pavel Ryabchuk
Scott E. Denmark, Pavel Ryabchuk, Hyung Min Chi, and Anastassia Matviitsuk
Trevor V. Nykaza, Julian C. Cooper, and Alexander T. Radosevich
Bryan J. Simmons, Melissa Ramirez, and Neil K. Garg
Saskia M. Engle, Takisha R. Kirkner, and Christopher B. Kelly
Xanath Ispizua-Rodriguez, Vinayak Krishnamurti, Mathew Coe, and G. K. Surya Prakash
Nana B. Agyemang and Ryan P. Murelli
Pablo Gabriel, Lan-Gui Xie, and Darren J. Dixon
Kyle M. Lambert, Austin W. Medley, Amy C. Jackson, Lauren E. Markham, and John L. Wood
Francesca M. Ippoliti, Joyann S. Barber, and Neil K. Garg
Subject Areas: Chemistry [PN]
