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Organic Syntheses, Volume 95
Brian M. Stoltz (Author)
9781119595397, Wiley
Hardback, published 14 June 2019
592 pages
22.9 x 15.8 x 3 cm, 0.816 kg
The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.
Copper and Secondary Amine-Catalyzed Pyridine Synthesis from O-Acetyl Oximes and α,β-Unsaturated Aldehydes 1 An Au/Zn-catalyzed Synthesis of N-Protected Indole via Annulation of N-Arylhydroxamic Acid and Alkyne 15 Preparation of Fac-Tris(2-Phenylpyridinato) Iridium(III) 29 Preparation of Cyclopent-2-enone Derivatives via the Aza-Piancatelli Rearrangement 46 Catalytic, Metal-Free Oxidation of Primary Amines to Nitriles 60 Copper-Catalyzed Enantioselective Hydroamination of Alkenes 80 Preparation of 6H-Benzo[c]chromen-6-one 97 Synthesis of N-Acyl Pyridinium-N-Aminides and Their Conversion to 4-Aminooxazoles via a Gold-Catalyzed Formal (3+2)-Dipolar Cycloaddition 112 Preparation of Solid Organozinc Pivalates and Their Reaction in Pd-Catalyzed Cross-Couplings 127 Enantioselective Synthesis of (S)-Ethyl 2-((tert-butoxycarbonyl)((tertbutyldimethylsilyl) oxy)amino)-4 oxobutanoate 142 Preparation of (S)-N-Boc-5-oxaproline 157 Syntheses of Substituted 2-Cyano-benzothiazoles 177 Preparation of N-(1,7,7-Trimethylbicyclo[2.2.1]heptan-2-ylidene) nitramide 192 Preparation of Alkyl Boronic Esters Using Radical-Polar Crossover Reactions of Vinylboron Ate Complexes 205 Preparation of (pin)B–B(dan) 218 Discussion Addendum for: Preparation of a Carbazole-Based Macrocycle Via Precipitation-Driven Alkyne Metathesis 231 Hydrodecyanation by a Sodium Hydride-Iodide Composite 240 Indole-Catalyzed Bromolactonization: Preparation of Bromolactone in Lipophilic Media 256 Discussion Addendum for: Stereoselective Synthesis of 3-Arylacrylates by Copper-Catalyzed Syn Hydroarylation [(E)-Methyl 3-phenyloct-2-enoate] 267 Modified McFadyen-Stevens Reaction for a Versatile Synthesis of Aromatic Aldehydes 276 Discussion Addendum for: Facile Syntheses of Aminocyclopropanes: N,N-Dibenzyl-N-(2-ethenylcyclopropyl)amine [(Benzenemethanamine, N-(2-ethenylcyclopropyl)-N-(phenylmethyl)) 289 (R)-2,2,2-Trichloro-1-phenylethyl (methylsulfonyl)oxycarbamate 310 Large Scale Synthesis of Enantiomerically Pure (S)-3-(4-Bromophenyl)- butanoic Acid 328 Preparation of Tributyl(iodomethyl)stannane 345 Stannylamine Protocol (SnAP) Reagents for the Synthesis of C–Substituted Morpholines from Aldehydes 357 Trimethylsilyldiazo[13C]methane: A Versatile 13C-Labelling Reagent 374 Stereoretentive Iron-catalyzed Cross-coupling of an Enol Tosylate with MeMgBr 403 Synthesis of Methyl 2-Bromo-3-oxocyclopent-1-ene-1-carboxylate 425 Discussion Addendum for: Preparation of (S)-tert-ButylPHOX and (S)-2-Allyl-2-Methylcyclohexanone 439 Synthesis of Acyl Derivatives of Cotarnine 455 Carbonyl-Olefin Metathesis for the Synthesis of Cyclic Olefins 472 Hexafluoro-2-propanol-promoted Intramolecular Friedel-Crafts Acylation 486 Discussion Addendum for: Preparation of the COP Catalysts: [(S)-COP-OAc]2, [(S)-COP-Cl]2, and (S)-COP-hfacac 500
Wei Wen Tan, Bin Wu, Ye Wei, and Naohiko Yoshikai
Xinpeng Cheng, Yanzhao Wang, and Liming Zha
Kip A. Teegardin and Jimmie D. Weaver
Meghan F. Nichol, Luis Limon, and Javier Read de Alaniz
Kyle M. Lambert, Sherif A. Eldirany, James M. Bobbitt, and William F. Bailey
Richard Y. Liu and Stephen L. Buchwald
Yang Wang, Yi Shi, and Vladimir Gevorgya
Matthew P. Ball-Jones and Paul W. Davies
Mario Ellwart, Yi-Hung Chen, Carl Phillip Tüllmann, Vladimir Malakhov, and Paul Knochel
Thibault J. Harmand, Claudia E. Murar, Hikaru Takano, and Jeffrey W. Bode
Claudia E. Murar, Thibault J. Harmand, Hikaru Takano, and Jeffrey W. Bode
Hendryk Würfel and Dörthe Jakobi
Emerson Teixeira da Silva, Adriana Marques Moraes, Adriele da Silva Araújo, and Marcus Vinícius Nora de Souza
Marvin Kischkewitz and Armido Studer
Hiroto Yoshida, Yuya Murashige, and Itaru Osaka
Christopher C. Pattillo, Morgan M. Cencer, and Jeffrey S. Moore
Guo Hao Chan, Derek Yiren Ong, and Shunsuke Chiba
Zhihai Ke, Tao Chen, and Ying-Yeung Yeung
Yoshihiko Yamamoto
Yuri Iwai and Jun Shimokawa
Armin de Meijere and Sergei I. Kozhushkov
Hélène Lebel, Henri Piras, and Johan Bartholoméüs
J. Craig Ruble, H. George Vandeveer, and Antonio Navarro
Michael U. Luescher, Chalupat Jindakun, and Jeffrey W. Bode
Michael U. Luescher, Chalupat Jindakun, and Jeffrey W. Bode
Chris Nottingham and Guy C. Lloyd-Jones
Takeshi Tsutsumi, Yuichiro Ashida, Hiroshi Nishikado, and Yoo Tanabe
Rama Rao Tata and Michael Harmata
Alexander W. Sun and Brian M. Stoltz
Laxmidhar Rout, Bibhuti Bhusan Parida, Ganngum Phaomei, Bertounesque Emmanuel, and Akhila Kumar Sahoo
Marc R. Becker, Katie A. Rykaczewski, Jacob R. Ludwig, and Corinna S. Schindler
Rakesh H. Vekariya, Matthew C. Horton, and Jeffrey Aubé
Jeffrey S. Cannon and Larry E. Overman
Subject Areas: Chemistry [PN]
