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Organic Syntheses, Volume 93
Huw M. L. Davies (Author), Erick M. Carreira (Author)
9781119349020, Wiley
Hardback, published 26 January 2018
464 pages
23.1 x 15.5 x 2.5 cm, 0.762 kg
The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.
DIBALH-Mediated Reductive Ring-Expansion Reaction of Cyclic Ketoxime 1 Preparation of 2-(2-(Dicyclohexylphosphino)phenyl)-1-methyl-1H-indole (CM-phos) 14 Synthesis of 5-(Hydroxymethyl)furfural (HMF) 29 Erratum for: Titanium-Mediated Addition of Silyl Dienol Ethers to Electrophilic Glycine: 4 Ketopipecolic Acid Hydrochloride 37 Nickel-Catalyzed Synthesis of Ketones from Alkyl Halides and Acid Chlorides: Preparation of Ethyl 4-Oxododecanoate 50 Trichloroboron-promoted Deprotection of Phenolic Benzyl Ether UsingPentamethylbenzene as a Non Lewis-Basic Cation Scavenger 63 Enantioselective Synthesis of α,α-Disubstituted Lactones via a Chiral Brønsted Acid-Catalyzed Intramolecular Cyclization 75 Enantioselective Synthesis of α-Bromonitroalkanes for Umpolung Amide Synthesis: Preparation of tert-Butyl ((1R)-1-(4-(benzyloxy)phenyl)-2-bromo-2-nitroethyl)carbamate 88 Synthesis of 1-Bromopyrene and 1-Pyrenecarbaldehyde 100 Intermolecular [2+2] Cycloaddition of Alkynes with Alkenes Catalyzed by Gold(I) 115 Photochemical Benzannulation of N-Phosphoryl Ynamides and α-Diazo Ketones in Continuous Flow 127 Trifluoromethylation of Aryl Iodides Catalyzed by the Copper(I)-Phen Complex 147 Copper-catalyzed Cyanation of Alkenyl Iodides 163 Visible Light Photocatalysis of Radical Cation Diels–Alder Cycloadditions: Preparation of Tris(2,2’-bipyrazyl) Ruthenium(II) Bis(tetrakis(3,5-bis(trifluoromethyl)phenyl)borate) 178 Preparation of Methyl 1,2,3,4-tetra-O-acetyl-β-D-glucopyranuronate 200 Preparation of 1,5-Dioxaspiro[5.5]undecan-3-one 210 Oxyboration: Synthesis of Borylated Benzofurans 228 Synthesis of 1-Iodopropyne 245 Potassium tert-Butoxide–Catalyzed Dehydrogenative Cross-Coupling of Heteroarenes with Hydrosilanes 263 Synthesis of α-Carboline 272 Synthesis of Methyl 1-Formylcyclopropanecarboxylate utilizing Ti-Claisen Condensation 286 Nickel-Catalyzed Suzuki–Miyaura Coupling in t-Amyl Alcohol for the Preparation of 5-(Furan-3-yl)pyrimidine 306 Preparation of (S)-Nonafluorobutanesulfinamide 319 Preparation of 1-Methylimidazole-N-oxide (NMI-O) 331 Palladium-Catalyzed Direct Amination of Allylic Alcohols at Room Temperature 341 Preparation of 1,1-Difluoroallenes by Difluorovinylidenation of Carbonyl Compounds 352 Rhodium-Catalyzed Addition of Carboxylic Acids to Terminal Alkynes towards Z-Enol Esters 367 Copper-Catalyzed Semi-Reduction of Alkynes 385 Synthesis of Cyclobutanes by Lewis Acid-Promoted Ketene-Alkene [2+2] Cycloadditions 401 Synthesis of 2,2-Dichloroimidazolidine-4,5-diones and their Application in Chlorodehydroxylation 413
Taku Imaizumi, Kentaro Okano, and Hidetoshi Tokuyama
Shun Man Wong, On Ying Yuen, Pui Ying Choy, Chau Ming So, and Fuk Yee Kwong
Svilen P. Simeonov, Jaime A. S. Coelho, and Carlos A. M. Afonso
Clarisse Mühlemann, Peter Hartmann, and Jean-Pierre Obrecht
Alexander C. Wotal, Donald C. Batesky, and Daniel J. Weix
Shun Okaya, Keiichiro Okuyama, Kentaro Okano, and Hidetoshi Tokuyama
Jennifer E. Wilent, Ghassan Qabaja, and Kimberly S. Petersen
Victoria T. Lim, Sergey V. Tsukanov, Amanda B. Stephens, and Jeffrey N. Johnston
Matthias Schulze, Alexander Scherer, Colin Diner, and Rik R. Tykwinski
M. Elena de Orbe and Antonio M. Echavarren
John M. Read, Yu-Pu Wang, and Rick L. Danheiser
Naoto Shimizu, Hideaki Kondo, Masahiro Oishi, Kenichi Fujikawa, Kazuki Komoda, and Hideki Amii
Antoine Nitelet, Sara Zahim, Cédric Theunissen, Alexandre Pradal, and Gwilherm Evano
Shane D. Lies, Shishi Lin, and Tehshik P. Yoon
Aisling Ní Cheallaigh, Garrett T. Potter, John M. Gardiner, and Gavin J. Miller
Robert A. Craig, II, Russell C. Smith, Beau P. Pritchett, Benzi I. Estipona, and Brian M. Stoltz
Darius J. Faizi, Nicole A. Nava, Mohammad Al-Amin, and Suzanne A. Blum
Samuel G. Bartko, James Deng, and Rick L. Danheiser
Anton A. Toutov, Wen-Bo Liu, Brian M. Stoltz, and Robert H. Grubbs
Linli He, Shawn P. Allwein, Benjamin J. Dugan, Kyle W. Knouse, Gregory R. Ott, and Craig A. Zificsak
Yuichiro Ashida, Satomi Kajimoto, Hidefumi Nakatsuji, and Yoo Tanabe
Liana Hie and Neil K. Garg
Apiwat Wangweerawong, Scott Kolmar, and Jonathan A. Ellman
James I. Murray and Alan C. Spivey
Bao Gao, Lixin Li, Guoying Zhang, and Hanmin Huang
Kohei Fuchibe, Masashi Abe, Ken Oh, and Junji Ichikawa
Stephanie Ganss, Julia Pedroni, Alexandre Lumbroso, Günther Leonhardt-Lutterbeck, Antje Meißner, Siping Wei, Hans-Joachim Drexler, Detlef Heller, and Bernhard Breit
Nick Cox, Hester Dang, Aaron M. Whittaker, and Gojko Lalic
Christopher M. Rasik, Eleni M. Salyers, and M. Kevin Brown
David Schilter and Christopher W. Bielawski
Subject Areas: Chemistry [PN]
