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Organic Syntheses, Volume 91
Kay M. Brummond (Edited by), KM Brummond (Author)
9781119054160, Wiley
Hardback, published 14 July 2015
416 pages
23.5 x 15.9 x 2.8 cm, 0.667 kg
The demand for synthetic procedures that can be duplicated may be less egregious today than in 1921, but there is still a need. To date, Organic Syntheses has filled this need with 90 volumes of "checked" experimentals; and with the culmination of Kay Brummond's term as a member of the editorial board, the addition of Volume 91.
Discussion Addendum: Resolution of 1,1'-Bi-2-Naphthol; (R)-(+)- and (S)-(-)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl(BINAP) 1 Discussion Addendum for: Practical Synthesis of Novel Chiral Allenamides: (R)-4-Phenyl-3-(1,2-propadienyl)oxazoldin-2-one 12 N-Carboxylated-2-substituted Indoles and 2,3-Disubstituted-2,3-dihydro-4-quinolones from 2-Alkynylbenzamides 27 Pd-Catalyzed External-CO-Free Carbonylation: Preparation of 2,4,6-Trichlorophenyl 3,4-Dihydronaphthalene-2-Carboxylate 39 Rhodium-Catalyzed Direct Amination of Arene C-H Bonds Using Azides as the Nitrogen Source 52 Synthesis of Alkynyliodonium Salts: Preparation of Phenyl (phenylethynyl)iodonium Trifluoroacetate 60 Palladium-catalyzed 1,4-Addition of Terminal Alkynes to Conjugated Enones 72 Cross-Coupling of Alkenyl/Aryl Carboxylates with Grignard Reagents via Fe-Catalyzed C-O Bond Activation 83 Preparation of 5-Hydroxycyclopentenones Via Conjugate Addition-Initiated Nazarov Cyclization 93 Synthesis of Arylboronic Pinacol Esters from Corresponding Arylamines 106 Preparation of Alkanesulfonyl Chlorides from S-Alkyl Isotghiourea Salts via N-Chlorosuccinimide Mediated Oxidative Chlorosulfonation 116 DABCO-bis(sulfur dioxide), DABSO, as an easy-to-handle source of SO2: Sulfonamide preparation 125 One-pot Preparation of (S)-N-[(S)-1-Hydroxy-4-metghyl-1,1-diphenylpentan-2-yl]pyrrolidine-2-carboxamide from L-Proline 137 Enantioselective Rhodium-Catalyzed [2+2+2] Cycloaddition of Pentenyl Isocyanate and 4-Ethynylanisole: Preparation and Use of Taddol-pyrrolidine Phosphoramidite 150 Synthesis and Use of a Trifluoromethylated Azomethine Ylide Precursor: Ethyl 1-Benzyl-trans-5-(trifluoromethyl)pyrrolidine-3-carboxylate 162 Enantioselective Organocatalytic-α-Arylation of Aldehydes 175 Synthesis of 4,5-Disubstituted 2-aminothiazoles from α,β-Unsaturated Ketones: Preparation of S-benzyl-4-methyl-2-aminothiazolium Hydrochloride salt 185 Sodium Methoxide-Catalyzed Direct Amidation of Esters 201 Synthesis of Tetrasubstituted 1H-Pyrazoles by Copper-mediated Coupling of Enaminones with Nitriles 211 Synthesis of 1,3-Dimethyl-3-(p-tolyl)-1H-pyrrolo[3,2-c]pyridin-2(3H)-one by Cu(II)-Mediated Direct Oxidative Coupling 221 Preparation of (R)-4-Cyclohexyl-2,3-butadien-1-ol 233 Discussion Addendum for: Formation of y-Keto Esters from β-Keto Esters: Methyl 5,5-dimethyl-4-oxohexanoate 248 Ni-catalyzed Reductive Cleavage of Methyl 3-Methoxy-2-Naphthoate 260 Indium-Catalyzed Heteroaryl-Heteroaryl Bond Formation through Nucleophilic Aromatic Substitution: Preparation of 2-Methyl-3-(thien-2-yl)-1H-indole 273 Synthesis of 2,3-Disubstituted Benzofurans by the Palladium-Catalyzed Coupling of 2-Iodoanisoles and Terminal Alkynes, Followed by Electrophilic Cyclization: 3-Iodo-2-phenylbenzofuran 283 Enantioselective Preparation of (S)-5-Oxo-5,6-dihydro-2H-oyran-2-yl Benzoate 293 Iron-Catalyzed Selective Conjugate Addition of Aryl Grignard Reagents to 2,4-Alkadienoates: tert-Butyl (Z)-5-Phenyl-3-hexenoate 307 3-Hydrixymethyl-3-phenylcyclopropene 322 Enantioselective Synthesis of α- and β-Boc-protected 6-Hydroxy-pyranones: Carbohydrate Building Blocks 338
David L. Hughes
Yong-Chua Teo and Richard P. Hsung
Noriko Okamoto, Kei Takeda, and Reiko Yanada
Hideyuki Konishi, Tsuyoshi Ueda, and Kei Manabe
Sae Hume Park, Yoosu Park, and Sukbok Chang
Luke I. Dixon, Michael A. Carroll, George J. Ellames and Thomas J. Gregson
Feng Zhou, Liang Chen and Chao-Jun Li
Bi-Jie Li, Xi-Sha Zhang and Zhang-Jie Shi
Joshua L. Brooks, Yu-Wen Huang, and Alison J. Frontier
Di Qiu, He Meng, Liang Jin, Shengbo Tang, Shuai Wang, Fangyang Mo, Yan Zhang and Jianbo Wang
Zhanhui Yang and Jiaxi Xu
Edward J. Emmett and Michael C. Willis
Wacharee Hamying, Nonognaphat Duangdee, and Albrecht Berkessel
Kevin M. Oberg, Timothy J. Martin, Mark Emil Oinen, Derek M. Dalton, Rebecca Keller Friedman, Jamie M. Neely, and Tomislav Rovis
Daniel M. Allwood, Duncan L. Browne and Steven V. Ley
Pernille H. Poulsen, Mette Overgaard, Kim L. Jensen and Kari Anker Jørgensen
Antonio Bermejo Gómez, Nanna Ahlsten, Ana E. Platero-Prats and Belen Martin-Matute
Kazushi Agura, Takashi Ohshima, Yukiko Hayashi, And Kazushi Mashima
Mamta Suri and Frank Glorius
Chandan Dey and E. Peter Kundig
Juntao Ye and Shengming
Yashoda M. D. Bhogadhi and Charles K. Zercher
Josep Cornella, Cayetana Zarate, and Ruben Martin
Yuta Nagase and Teruhisa Tsuchimoto
Tuanli Yao, Dawei Yue, and Richard C. Larock
Tamas Benkovics, Adrian Ortiz, Zhiwei Guo, Animesh Goswami and Prashant Deshpande
Takeshi Hata, Hideyuki Goto, Tomofumi Yokomizo, and Hirokazu Urabe
Ramajeyam Selvaraj, Srinvasa R. Chintala, Michael T. Taylor and Joseph M. Fox
Sumit O. Bajaj, Jamison R. Farnsworth and George A. O'Doherty
Subject Areas: Chemistry [PN]
