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Organic Syntheses, Volume 101
Sarah E. Reisman (Edited by)
9781394407286, Wiley
Hardback, published 7 January 2026
624 pages
23.1 x 16.3 x 3.8 cm, 0.794 kg
The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.
Synthesis of Secondary Benzylic Alcohols by Reductive Arylation of Aldehydes: α-Phenyl-6-quinolinemethanol 1 Synthesis of Deuterated 1H-Indole-3-carboxaldehyde via Catalytic Vilsmeier-Haack Reaction 21 Metal-Free Aziridination of Alkenes with Free Amines by Thianthrenation 34 Cobalt-catalyzed Radical Olefin Isomerization: Retrocycloisomerization of (−)-Caryophyllene Oxide to (−)-Humulene Oxide II 51 Preparation of Radical Clocks Bearing Carbonyl Groups: Synthesis of N-Methoxy-N-methylspiro[cyclopropane 1,9'-fluorene]-2-carboxamide 61 Discussion Addendum for: Mild Conversion of Tertiary Amides to Aldehydes Using Cp2Zr(H)Cl (Schwartz's Reagent) 81 Synthesis of 5-(1-Diazo-2-ethoxy-2-oxoethyl) dibenzo- [b,d]thiophenium Triflate 109 Tandem Fragmentation/Olefination for Production of Neopentylene-Tethered 1,6-Enynes from Dimedone 124 Nickel-catalyzed Amination of Aryl Chlorides 150 Difluoromethylation of Phenols 164 Intramolecular Coupling for General Synthesis of Backbone Substituted Bicyclo[1.1.1]pentyl Boronates 181 Chromatography-Free and Chlorinated Solvent-Free Preparation of 2,5-dibromohexanediamide (DBHDA) 207 Platinum-Catalyzed Enantioselective Diboration of Monosubstituted Alkenes 229 Preparation of 2-Chloro-1-(1-ethoxyvinyl)pyridinium Triflate 242 One-pot Synthesis of Alkynes from Esters via a Tandem Reduction-Ohira-Bestmann Reaction 258 Synthesis of S,S-Di(pyridin-2-yl)carbonodithioate (DPDTC) for the Reduction of Carboxylic Acids 274 Discussion Addendum for: Palladium-Catalyzed Dehydrative Allylation of Hypophosphorous Acid with Allylic Alcohols. Preparation of Cinnamyl-H-Phosphinic Acid 295 Synthesis of Benzyl- -Truxinate via Enantioselective [2+2] Photocycloaddition 309 Hydration of Nitriles to Primary Amides Enabled by the Ghaffar-Parkins Catalyst 327 Preparation of Highly Reactive Lithium Metal Dendrites and the Synthesis of (Trimethylsilyl)methyllithium 342 Synthesis of 3,3-Dimethyl-nitroso-2,3- dihydrobenzo[d]- isothiazole 1,1-dioxide (NO-1) 366 α-Arylation of N-Boc Pyrrolidine 382 Preparation of S-Methyl Methanethiosulfonate from Dimethyl Sulfoxide Initiated by Oxalyl Chloride 395 Synthesis of 3-Azabicyclo[3.2.0]heptane Hydrochloride 410 Discussion Addendum for: Preparation of 2-(2-(Dicyclohexylphosphino)phenyl)-1-methyl-1H-indole (CM-phos) 423 Discussion Addendum for: Palladium-catalyzed Buchwald-Hartwig Amination and Suzuki-Miyaura Cross-coupling Reaction of Aryl Mesylates 438 Oxygen-Free Alkene Hydration Using Nitroarenes: Diastereoselective Hydration of Cholesteryl Acetate 460 Nitrosation of Diphenylamine with 3,3-Dimethyl-2- Nitroso-2,3- Dihydrobenzo[d]isothiazole 1,1-dioxide (NO-1) 478 Hydrodealkenylative Cleavage of C(sp3)–C(sp2) Bonds: Preparation of (1S, 3R)-3-Methylcyclohexan-1-ol 488 Discussion Addendum for: Dipeptide Syntheses via Activated -Amino Esters 508 meta-C–H Halogenation of Pyridines, Quinolines, and Isoquinolines: meta-Chlorination of 2-Phenylpyridine 524 Synthesis of 4-(2,2-Difluorovinyl)benzonitrile through a Wittig-type Olefination of 4-Formylbenzonitrile 542
Gilian T. Thomas, Eric S. Isbrandt, and Stephen G. Newman*
Jing Xue, Yushan Zhang, Bing Zhong, and Jin-Dong Yang*
Ming-Shang Liu and Wei Shu
Eleanor M. Landwehr and Ryan A. Shenvi*
Nicole D. Bartolo, Ryan N. Robson, Collin H. Witt, and K. A. Woerpel*
Narsihmulu Cheryala, Rui Shi, Shelby Mcguire, Naresh Gantasala, Nagarjun Reddy Vantaddu, Ravikrishna Dada, Nan Wang, Shameem S. Syeda, Hira Khalid, and Gunda I. Georg*
Brigitte Worbs, Sven Timmann, Feng Peng, Ralph Zhao, and Manuel Alcarazo*
Kh Tanvir Ahmed, A. C. Martin, Gabriella O. Wabler, Kristen S. Nerbecki, and Gregory B. Dudley*
Zachary G. Walters, Daniel W. Turner, and Neil K. Garg*
Allison T. Hands, Zachary G. Walters, Jacob P. Sorrentino, and Neil K. Garg*
Jet Tsien, Yangyang Yang, René García-Del Valle, Jonathan M. E. Hughes, Byron K. Peters, Rohan R. Merchant, and Tian Qin*
Ben Bower, Sébastien R. G. Galan, and Benjamin G. Davis*
Chenpeng Gao, Paul S. Lee, and James P. Morken*
John P. Frank, William R. Strutton, Joel K. A. Adade, and Max M. Majireck*
Cholapat Varongchayakul and Rick L. Danheiser *
Karthik S. Iyer, Jordan R. Yirak, Hubert Muchalski,* and Bruce H. Lipshutz*
Karla Bravo-Altamirano and Jean-Luc Montchamp*
Rodrigo Villanueva, Ellie F. Plachinski, and Tehshik P. Yoon*
Daniel W. Turner, Allison T. Hands, and Neil K. Garg*
Raquel M. Gonzalez, Han-Hsiang Hsu, and Andy A. Thomas*
Keerthana Chakkanalil, Pravien S. Rajaram, and Ryan D. Baxter*
Kevin Campos,* Melissa Howard, Hengyu Li, and Feng Peng
Xixuan Zhao, Shuai Peng, Hao Wang, Shuai Huang, Baoguo Sun, Hongyu Tian,* and Sen Liang*
Carl M. F. Mansson and Noah Z. Burns*
Cheuk Lam Cheung, Pui Ying Choy,* Man Ho Tse, and Fuk Yee Kwong*
Yu Kiu Lau, Man Ho Tse, Pui Ying Choy,* and Fuk Yee Kwong*
Jonas Elfert, Anup Bhunia, and Armido Studer*
Pravien S. Rajaram, Keerthana Chakkanalil, and Ryan D. Baxter*
Brady W. Dehnert and Ohyun Kwon*
Jean-Marc Campagne* and Renata Marcia de Figueiredo*
Pengwei Xu and Armido Studer*
Andrew J. Intelli, Jacob P. Sorrentino, and Ryan A. Altman*
Subject Areas: Chemistry [PN]
