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Glow Discharge Plasmas in Analytical Spectroscopy
R. Kenneth Marcus (Edited by), RK Marcus (Author), José A. C. Broekaert (Edited by)
9780471606994, Wiley
Hardback, published 27 November 2002
512 pages
28 x 22.5 x 0.4 cm, 0.822 kg
"...very valuable for those interested in this rapidly expanding and diagnostically important area."
Journal of the American Chemical Society
Vol. 125, NO. 39
Gegenstand des Bandes ist die Anwendung von Glimmentladungsplasmen in der analytischen Spektroskopie, insbesondere der Atomemissions-Spektroskopie und Massenspektrometrie.
- Sammlung von Beiträgen international renommierter Fachleute
- Herausgeber gehört zu den bekanntesten Persönlichkeiten seines Faches
- einziges Buch auf dem Markt, das einen wirklich umfassenden Überblick über die aktuelle Forschung auf diesem Gebiet gibt
- behandelt sowohl AES als auch MS mit Glimmentladungsplasmen
Preface xi List of Contributors xiii 1 Introduction 1 1.1 Rationale 1 1.2 Glow Discharge Devices: Basic Operating Principles 3 1.3 Glow Discharge Devices: Scope of Application 6 1.4 Volume Outline 7 1.5 References 12 2 Optical Emission Spectrometry with Glow Discharges 15 2.1 Introduction 15 2.2 Glow Discharges 16 2.3 Atomic Emission Spectrometry 36 2.4 Material Ablation 49 2.5 Analyses with Glow Discharge Atomic Emission Spectrometry 55 2.6 Other Methods of Analysis and Outlook 63 2.7 References 67 3 Mass Spectrometry of Glow Discharges 71 3.1 Introduction 71 3.2 Fundamentals of Mass Spectrometry 75 3.3 Instrumentation 82 3.4 Qualitative Considerations 91 3.5 Quantitative Analysis 92 3.6 Conclusions 95 3.7 References 95 4 Radio Frequency Glow Discharges 97 4.1 Introduction 97 4.2 Radio Frequency Glow Discharge (rf-GD) Operation Principles 99 4.3 Comparisons with dc-Powered Glow Discharge Sources 101 4.4 Instrumentation 106 4.5 Analytical Applications 112 4.6 Summary 136 4.7 References 136 5 Depth Profile Analysis 141 5.1 Introduction 141 5.2 Instrumentation 142 5.3 Practical Aspects and Results 144 5.4 Conclusions 153 5.5 References 154 6 Numerical Modeling of Analytical Glow Discharges 155 6.1 Introduction 155 6.2 Description of the Models 157 6.3 Results and Discussion 170 6.4 Conclusion 202 6.5 References 203 7 Application of Glow Discharge Optical Emission Spectrometry in the Steel Industry 207 7.1 Introduction 207 7.2 Measurement Traceability of Coating Weight and Chemical Composition by GD-OES 208 7.3 Method of Coating Analysis by GD-OES 209 7.4 Depth Profiles of Coatings by GD-OES 213 7.5 Factors Affecting Depth Profiles 217 7.6 Validation and Verification of Calibration Graphs 225 7.7 References 229 8 Surfaces, Thin Films and Coatings 231 8.1 Introduction 231 8.2 Surfaces 232 8.3 Thin Films 238 8.4 Coatings 243 8.5 Conclusions 251 8.6 Acknowledgements 251 8.7 References 251 9 Comparison of Glow Discharge Atomic Spectrometry with Other Surface Analysis Methods 253 9.1 Introduction 253 9.2 Surface Analysis Methods Competitive with Glow Discharge Spectrometry 256 9.3 Analytical Examples 263 9.4 References 272 10 Analysis of Samples of Nuclear Concern with Glow Discharge Atomic Spectrometry 273 10.1 Introduction 273 10.2 Instrumentation 274 10.3 Practical Aspects and Results 277 10.4 Conclusions 288 10.5 Acknowledgements 289 10.6 References 290 11 Analysis of Nonconducting Materials by dc Glow Discharge Spectrometry 293 11.1 Introduction 293 11.2 Use of a Conducting Host Matrix 294 11.3 Use of a Conducting Secondary Cathode 301 11.4 Conclusion 311 11.5 References 314 12 Standards and Reference Materials for Glow Discharge Spectroscopies 317 12.1 Introduction 317 12.2 Practical Aspects 318 12.3 Conclusions 331 12.4 References 332 13 Analysis of Liquid Samples Using Glow Discharge Spectroscopies 335 13.1 Introduction 335 13.2 Instrumentation 336 13.3 Practical Aspects and Applications 341 13.4 References 360 14 GC Speciation with GDMS Detection 363 J. A. Caruso and L. Milstein 14.1 Introduction 363 14.2 Elemental Speciation 364 14.3 Instrumentation 364 14.4 Practical Aspects and Results 370 14.5 Conclusions 378 14.6 References 379 15 Glow Discharge Atomic Emission Spectrometry for the Analysis of Gases and as an Alternative Gas Chromatographic Detector 381 15.1 Introduction 381 15.2 Instrumentation for the Analysis of Gases and Gas Chromatographic Detection by GD-AES 386 15.3 Practical Aspects and Results 392 15.4 Conclusions 399 15.5 References 399 16 Low-pressure Inductively Coupled Plasmas 401 16.1 Introduction 401 16.2 Fundamentals 403 16.3 Instrumentation 407 16.4 Practical Aspects and Results 416 16.5 Conclusions 430 16.6 References 430 17 Multidimensional Ionization Sources for Plasma-source Mass Spectrometry 435 17.1 Introduction 435 17.2 Tandem Sources in PSMS 437 17.3 Multipurpose Ionization Sources for PSMS 441 17.4 Conclusions 463 17.5 Acknowledgments 463 17.6 References 464 Index 469
R. K. Marcus and J. A. C. Broekaert
J. A. C. Broekaert
W. W. Harrison, C. Yang and E. Oxley
R. K. Marcus
A. Bengtson
A. Bogaerts and R. Gijbels
K. Kakita
R. Payling, P. Chapon, K. Shimizu, R. Passetemps, A. Jadin, Y. Bourgeois, K. Crener, M. Aeberhard and J. Michler
K. Wagatsuma
M. Betti
A. Bogaerts, W. Schelles and R. Van Grieken
M. R. Winchester
R. K. Marcus
R. Pereiro, N. G. Orellana-Velado and A. Sanz-Medel
H. Evans
J. P. Guzowski, Jr and G. M. Hieftje
Subject Areas: Chemistry [PN]
