Chemical Separations
Principles, Techniques and Experiments

Clifton E. Meloan (Author)

9780471351979, Wiley

Hardback, published 3 November 1999

768 pages
28.8 x 21.5 x 4.2 cm, 1.996 kg

"...the book provides a good balance between techniques relevant for chemical separation and experimental work." (The Analyst, 18th August 2000)

Laborhandbuch und Nachschlagewerk zugleich! Prinzipien, Ausrustung und technische Details der wichtigsten Trennverfahren werden aus der Sicht der praktischen Anwendung beschrieben, wobei der Autor mit einem Minimum an mathematischen Formeln auskommt. Anhand von 59 Beispielexperimenten wird das richtige Vorgehen demonstriert. Mit diesem Buch lernen auch Anfanger auf dem Gebiet der chemischen Analytik, mit Hilfe kommerzieller Produkte und bewahrter Verfahren exakte Ergebnisse zu erzielen. (04/00)

SEPARATIONS INVOLVING PHASE CHANGES.

Volatilization.

Zone Melting.

Distillation: General Information.

Azeotropic and Extractive Distillations.

Steam and Immiscible Solvents Distillation.

Vacuum Distillation.

Molecular Distillation and Sublimation.

Lyophilization (Freeze Drying).

SEPARATIONS INVOLVING EXTRACTION.

Extraction: General Concepts.

Continuous Extraction.

Countercurrent (Extraction) Chromatography: The Ito Coil-Planet Centrifugal Extractor.

Solid Phase Extraction.

Supercritical Fluid Extraction.

SEPARATIONS INVOLVING CHROMATOGRAPHY.

Chromatography: General Theory.

Displacement and Multiple Column Partition Chromatography.

Affinity Chromatography.

Size Exclusion Chromatography (Gel Filtration;
Gel Permeation).

Flash Chromatography.

High Performance Liquid Chromatography (HPLC).

Gas-Liquid Chromatography.

Paper Chromatography.

Thin Layer Chromatography.

SEPARATIONS INVOLVING ION EXCHANGE RESINS.

Ion Exchange.

Ion Chromatography.

Ion Retardation, Ion Exclusion, and Ligand Exchange.

SEPARATIONS INVOLVING ELECTRIC FIELDS.

Electrodeposition.

Electrophoresis--General.

Immunoelectrophoresis.

Polyacrylamide Gel Disc Electrophoresis.

Ion Focusing, SDS, and Two-Dimensional Electrophoresis.

Capillary Zone Electrophoresis.

Field Flow Fractionation.

SEPARATIONS INVOLVING FLOTATION.

Purge and Trap and Dynamic Headspace Analysis

Foam Fractionation, Gas-, and Liquid-Assisted Flotation.

SEPARATIONS INVOLVING MEMBRANES.

Osmosis and Reverse Osmosis.

Dialysis and Electrodialysis

Filtering and Sieving.

SEPARATIONS INVOLVING MISCELLANEOUS TECHNIQUES.

Density Gradients.

Centrifugation.

Masking and Sequestering Agents.

Solubility.

Gas Analysis by Portable Orsat.

Appendices.

Index.

Subject Areas: Chemistry [PN]