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Advanced ESR Methods in Polymer Research
Shulamith Schlick (Edited by), S Schlick (Author)
9780471731894, Wiley
Hardback, published 3 October 2006
368 pages
24.1 x 16.3 x 2.3 cm, 0.63 kg
A definitive work on ESR and polymer science by today's leading authorities
The past twenty years have seen extraordinary advances in electron spin resonance (ESR) techniques, particularly as they apply to polymeric materials. With contributions from over a dozen of the world's top polymer scientists, Advanced ESR Methods in Polymer Research is the first book to bring together all the current trends in this exciting field into one comprehensive reference.
Part I establishes the fundamentals of ESR, from experimental techniques to data analysis, and serves as a valuable overview for the beginning ESR student. Part II introduces the broad range of ESR applications to polymeric systems, including living radical polymerization, block copoly-mers, polymer solutions, ion-containing polymers, polymer lattices, membranes in fuel cells, degradation, polymer coatings, dendrimers, and conductive polymers. By exposing readers to the great potential of ESR, the authors hope to encourage more extensive application of these methods.
PREFACE ix ABOUT THE EDITOR xi CONTRIBUTORS xiii PART I ESR FUNDAMENTALS 1 1 Continuous-Wave and Pulsed ESR Methods 3 2 Double Resonance ESR Methods 25 3 Calculating Slow-Motion ESR Spectra of Spin-Labeled Polymers 53 4 ESR Imaging 85 PART II ESR APPLICATIONS 99 5 ESR Study of Radicals in Conventional Radical Polymerization Using Radical Precursors Prepared by Atom Transfer Radical Polymerization 101 6 Local Dynamics of Polymers in Solution by Spin-Label ESR 133 7 Site-Specific Information on Macromolecular Materials by Combining CW and Pulsed ESR on Spin Probes 165 8 ESR Methods for Assessing the Stability of Polymer Membranes Used in Fuel Cells 197 9 Spatially Resolved Degradation in Heterophasic Polymers From 1D and 2D Spectral–Spatial ESR Imaging Experiments 229 10 ESR Studies of Photooxidation and Stabilization of Polymer Coatings 255 11 Characterization of Dendrimer Structures by ESR Techniques 279 12 High-Field ESR Spectroscopy of Conductive Polymers 307 INDEX 339
Gunnar Jeschke and Shulamith Schlick
Gunnar Jeschke
Keith A. Earle and David E. Budil
Shulamith Schlick
Atsushi Kajiwara and Krzysztof Matyjaszewski
Jan PilarB
Gunnar Jeschke
Emil Roduner and Shulamith Schlick
Shulamith Schlick and Krzysztof Kruczala
David R. Bauer and John L. Gerlock
M. Francesca Ottaviani and Nicholas J. Turro
Victor I. Krinichnyi
Subject Areas: Chemistry [PN]
