{"product_id":"x-ray-structure-determination-a-practical-guide-hardback-9780471607113","title":"X-Ray Structure Determination; A Practical Guide (Hardback) 9780471607113","description":"\u003cfont face=\"Georgia\"\u003e\r\n\u003cp\u003e\u003cfont size=\"6\"\u003eX-Ray Structure Determination\u003c\/font\u003e\u003cbr\u003e\r\n\u003cfont size=\"5\"\u003eA Practical Guide\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\r\n\r\n\r\n\u003cp\u003e\u003cfont size=\"4\"\u003eGeorge H. Stout (Author), Lyle H. Jensen (Author)\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e9780471607113, Wiley\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003eHardback, published 21 June 1989\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e480 pages\u003cbr\u003e24.2 x 16.1 x 4.1 cm, 0.907 kg\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\r\n\r\n\r\n\r\n\u003cp align=\"justify\"\u003e\u003cstrong\u003e\u003cfont size=\"3\"\u003eClosely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.\u003c\/font\u003e\u003c\/strong\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003ePRELIMINARY STAGES.\u003cbr\u003e \u003cbr\u003e X-Rays.\u003cbr\u003e \u003cbr\u003e Diffraction of X-Rays.\u003cbr\u003e \u003cbr\u003e Crystals, Symmetry, and Space Groups.\u003cbr\u003e \u003cbr\u003e Crystals and Their Properties.\u003cbr\u003e \u003cbr\u003e Geometric Data Collection.\u003cbr\u003e \u003cbr\u003e Intensity Data Collection.\u003cbr\u003e \u003cbr\u003e Data Reduction.\u003cbr\u003e \u003cbr\u003e Theory of Structure Factors and Fourier Syntheses.\u003cbr\u003e \u003cbr\u003e Calculation of Structure Factors and Fourier Syntheses.\u003cbr\u003e \u003cbr\u003e THE PHASE PROBLEM.\u003cbr\u003e \u003cbr\u003e The Phase Problem.\u003cbr\u003e \u003cbr\u003e Direct Methods.\u003cbr\u003e \u003cbr\u003e Patterson Methods.\u003cbr\u003e \u003cbr\u003e Heavy Atom Methods.\u003cbr\u003e \u003cbr\u003e Search Methods.\u003cbr\u003e \u003cbr\u003e Completing the Structure.\u003cbr\u003e \u003cbr\u003e REFINEMENT AND RESULTS.\u003cbr\u003e \u003cbr\u003e Refinement of Crystal Structures.\u003cbr\u003e \u003cbr\u003e Random and Systematic Errors.\u003cbr\u003e \u003cbr\u003e Derived Results.\u003cbr\u003e \u003cbr\u003e Ambiguities and Uncertainties.\u003cbr\u003e \u003cbr\u003e Appendices.\u003cbr\u003e \u003cbr\u003e Index.\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003eSubject Areas: Chemistry [\u003ca title=\"See our other books on Chemistry\" href=\"https:\/\/freshlyprintedbooks.co.uk\/search?q=%22Chemistry%20%5BPN%5D%22\"\u003ePN\u003c\/a\u003e]\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\r\n\u003c\/font\u003e","brand":"Wiley-Interscience","offers":[{"title":"Brand New","offer_id":52507197604120,"sku":"9780471607113","price":150.39,"currency_code":"GBP","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0730\/2037\/5320\/files\/9780471607113.jpg?v=1786438995","url":"https:\/\/freshlyprintedbooks.co.uk\/products\/x-ray-structure-determination-a-practical-guide-hardback-9780471607113","provider":"Freshly Printed Books","version":"1.0","type":"link"}