{"product_id":"organic-syntheses-collective-volume-6-hardback-9780471852438","title":"Organic Syntheses, Collective Volume 6 (Hardback) 9780471852438","description":"\u003cfont face=\"Georgia\"\u003e\r\n\u003cp\u003e\u003cfont size=\"6\"\u003eOrganic Syntheses, Collective Volume 6\u003c\/font\u003e\u003cbr\u003e\r\n\r\n\r\n\r\n\r\n\r\n\u003c\/p\u003e\n\u003cp\u003e\u003cfont size=\"4\"\u003eWayland E. Noland (Edited by), WE Noland (Author)\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e9780471852438, Wiley\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003eHardback, published 30 April 1988\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e1234 pages\u003cbr\u003e23.5 x 15.9 x 6.2 cm, 1.642 kg\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\r\n\r\n\r\n\r\n\u003cp align=\"justify\"\u003e\u003cstrong\u003e\u003cfont size=\"3\"\u003eContains the procedures previously published in annual volumes 50-59, revised and updated where necessary. Efforts have been made to standardize the style of experimental procedures and the presentation of spectroscopic data. Increasing emphasis on the toxicology of organic compounds has led to the inclusion of additional hazard warnings, particularly for benzene, hexamethylphosphoric triamide (HMPA), and methyl iodide at the many places where they appear. Some experimental procedures have been improved, references have been added, and the index has been greatly expanded and simultaneously consolidated for efficient and easy use.\u003c\/font\u003e\u003c\/strong\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e[The numbers in parentheses refer to the annual volume (in boldface type) and page number where each procedure first appeared]  \u003cp\u003eAcylamidoalkyl Acetophenones from Substituted Phenethylamines: 2-(2-Acetamidoethyl)-4,5-dimethoxyacetophenone … (56, 3)\u003c\/p\u003e \u003cp\u003eThiol Protection with the Acetamidomethyl Group: S-Acetamidomethyl-l-cysteine Hydrochloride … (59, 190)\u003c\/p\u003e \u003cp\u003eAcetic Formic Anhydride … (50, 1)\u003c\/p\u003e \u003cp\u003eAcetone Hydrazone … (50, 3)\u003c\/p\u003e \u003cp\u003ePreparation of Hydrazones: Acetophenone Hydrazone … (50, 102)\u003c\/p\u003e \u003cp\u003e3β-Acetoxy-5α-cyanocholestan-7-one … (52, 100)\u003c\/p\u003e \u003cp\u003ep-Acetyl-α-bromohydrocinnamic Acid … (51, 1)\u003c\/p\u003e \u003cp\u003eα,β-Dehydrogenation of β-Dicarbonyl Compounds by Selenoxide Elimination: 2-Acetyl-2-cyclohexen-1-one … (59, 58)\u003c\/p\u003e \u003cp\u003e2-Acetyl-1,3-cyclopentanedione … (52, 1)\u003c\/p\u003e \u003cp\u003e3-Acetyl-2,4-dimethylfuran … (53, 1)\u003c\/p\u003e \u003cp\u003e2-Acetyl-6-methoxynaphthalene … (53, 5)\u003c\/p\u003e \u003cp\u003eCopper Catalyzed Arylation of β-Dicarbonyl Compounds: 2-(1-Acetyl-2-oxopropyl)benzoic Acid … (58, 52)\u003c\/p\u003e \u003cp\u003e5-Acetyl- 1,2,3,4,5-pentamethylcyclopentadiene … (56, 1)\u003c\/p\u003e \u003cp\u003e2-Adamantanecarbonitrile … (57, 8)\u003c\/p\u003e \u003cp\u003eTertiary Alcohols from Hydrocarbons by Ozonation on Silica Gel: 1-Adamantanol … (59, 176)\u003c\/p\u003e \u003cp\u003eAdamantanone … (53, 8)\u003c\/p\u003e \u003cp\u003eEnone Reduction-Enolate Alkylation Sequence: 2-Allyl-3-methylcyclohexanone … (56, 52)\u003c\/p\u003e \u003cp\u003ePreparation of N-Aminoaziridines: trans-1-Amino-2,3-diphenylaziridine, 1-Amino-2-phenylaziridine, and 1-Amino-2-phenylaziridinium Acetate … (55, 114)\u003c\/p\u003e \u003cp\u003eReduction of Ketones by Use of the Tosylhydrazone Derivatives: Androstan-17β-Ol … (52, 122)\u003c\/p\u003e \u003cp\u003eAldehydes from 4,4-Dimethyl-2-oxazoline and Grignard Reagents: o-Anisaldehyde … (54, 42)\u003c\/p\u003e \u003cp\u003e[18]Annulene … (54, 1)\u003c\/p\u003e \u003cp\u003eAzetidine … (53, 13)\u003c\/p\u003e \u003cp\u003eAzoethane … (52, 11)\u003c\/p\u003e \u003cp\u003eDiels-Alder Addition of Perchlorobenzyne: Benzobarrelene … (59, 71)\u003c\/p\u003e \u003cp\u003eBenzocyclopropene … (55, 12)\u003c\/p\u003e \u003cp\u003eα-Chlorination of Carboxylic Acids Mediated by Chlorosulfonic Acid: \u0026amp;phis;-Benzoylamino-α-chlorocaproic Acid … (59, 20)\u003c\/p\u003e \u003cp\u003e1-N-Acylamino-1,3-dienes from 2,4-pentadienoic Acids by the Curtius Rearrangement: Benzyl trans-1,3-Butadiene-1-carbamate … (59, 1)\u003c\/p\u003e \u003cp\u003eBenzyl Chloromethyl Ether … (52, 16)\u003c\/p\u003e \u003cp\u003e1-Benzylindole … (54, 58)\u003c\/p\u003e \u003cp\u003eN-Alkylindoles from the Alkylation of Sodium Indolide in Hexamethylphosphoric Triamide: 1-Benzylindole … (54, 60)\u003c\/p\u003e \u003cp\u003e3-Alkylated and 3-Acylated Indoles from a Common Precursor: 3-Benzylindole and 3-Benzoylindole … (56, 8)\u003c\/p\u003e \u003cp\u003eAlkylation of Isoquinolines via 2-Benzoyl-1,2-dihydroisoquinaldonitriles: 1-Benzylisoquinoline … (56, 19)\u003c\/p\u003e \u003cp\u003eThe Formation and Alkylation of Specific Enolate Anions from an Unsymmetrical Ketone: 2-Benzyl-2-methylcyclohexanone and 2-Benzyl-6-methylcyclohexanone … (52, 39)\u003c\/p\u003e \u003cp\u003eSulfide Synthesis: Benzyl Sulfide … (58, 138)\u003c\/p\u003e \u003cp\u003eBicyclo[1.1.0]butane … (51, 55)\u003c\/p\u003e \u003cp\u003eBoranes in Functionalization of Dienes to Cyclic Ketones: Bicyclo[3.3.1]nonan-9-one … (58, 24)\u003c\/p\u003e \u003cp\u003eBicyclo[3.2.1]octan-3-one … (51, 60)\u003c\/p\u003e \u003cp\u003eBicyclo[2.1.0]pent-2-ene … (55, 15)\u003c\/p\u003e \u003cp\u003eDehydroxylation of Phenols; Hydrogenolysis of Phenolic Ethers: Biphenyl … (51, 82)\u003c\/p\u003e \u003cp\u003eControlled-Potential Electrolytic Reduction: 1,1-Bis(bromomethyl)cyclopropane … (52, 22)\u003c\/p\u003e \u003cp\u003eBis(trifluoromethyl)diazomethane … (50, 6)\u003c\/p\u003e \u003cp\u003eBis[2,2,2-trifluoro-1-phenyl-1-(trifluoromethyl)ethoxy] Diphenyl Sulfurane … (57, 22)\u003c\/p\u003e \u003cp\u003eAcyloin Condensation in which Chlorotrimethylsilane is Used as a Trapping Agent: 1,2-Bis(trimethylsilyloxy)cyclobutene and 2-Hydroxycyclobutanone … (57, 1)\u003c\/p\u003e \u003cp\u003e2-Bornene … (51, 66)\u003c\/p\u003e \u003cp\u003eSelective α-Bromination of an Aralkyl Ketone with Phenyltrimethylammonium Tribromide: 2-Bromoacetyl-6-methoxynaphthalene and 2,2-Dibromoacetyl-6-methoxynaphthalene … (53, 111)\u003c\/p\u003e \u003cp\u003eMercury(II) Oxide-Modified Hunsdiecker Reaction: 1-Bromo-3-chlorocyclobutane … (51, 106)\u003c\/p\u003e \u003cp\u003epara-Bromination of Aromatic Amines: 4-Bromo-N,N-dimethyl-3-(trifluoromethyl)aniline … (55, 20)\u003c\/p\u003e \u003cp\u003eBromohydrins from Alkenes and N-Bromosuccinimide in Dimethyl Sulfoxide; erythro-2-Bromo-1,2-diphenylethanol … (59, 16)\u003c\/p\u003e \u003cp\u003eChain Elongation of Alkenes via gem-Dihalocyclopropanes: 2-Bromo-3,3-diphenyl-2-propen-1-yl acetate … (56, 32)\u003c\/p\u003e \u003cp\u003e2-Bromohexanoyl Chloride … (55, 27)\u003c\/p\u003e \u003cp\u003e1-Bromo-3-methyl-2-butanone … (55, 24)\u003c\/p\u003e \u003cp\u003etrans, trans-1,3-Butadiene-1,4-diyl Diacetate … (50, 24)\u003c\/p\u003e \u003cp\u003eA New Reagent for tert-Butoxycarbonylation: 2-tert-Butoxycarbonyloxyimino-2-phenylacetonitrile … (59, 95)\u003c\/p\u003e \u003cp\u003etert-Butoxycarbonyl-l-proline … (53, 25)\u003c\/p\u003e \u003cp\u003etert-Butyl Azidoformate … (50, 9; 57, 122)\u003c\/p\u003e \u003cp\u003etert-Butylcyanoketene … (55, 32)\u003c\/p\u003e \u003cp\u003ecis-4-tert-Butylcyclohexanol … (50, 13)\u003c\/p\u003e \u003cp\u003ePolymeric Carbodiimide. Moffat Oxidation: 4-tert-Butylcyclohexanone … (56, 99)\u003c\/p\u003e \u003cp\u003eOxidation of Alcohols by Methyl Sulfide- N-Chlorosuccinimide- Triethylamine: 4-tert-Butylcyclohexanone … (58, 122)\u003c\/p\u003e \u003cp\u003e2-tert-Butyl-1,3-diaminopropane … (53, 21)\u003c\/p\u003e \u003cp\u003ePhotochemical Ring-Contraction of 2-Ethoxypyrrolin-5-ones to Cyclopropanone Derivatives: tert-Butyl N-(1-Ethoxycyclopropyl)carbamate … (59, 132)\u003c\/p\u003e \u003cp\u003ePhase-Transfer Hofmann Carbylamine Reaction: tert-Butyl Isocyanide … (55, 96)\u003c\/p\u003e \u003cp\u003eSulfide Synthesis in Preparation of Unsymmetrical Dlalkyl Disulfides: sec-Butyl Isopropyl Disulfide … (58, 147)\u003c\/p\u003e \u003cp\u003e3-Butyl-2-Methylhept-1-en-3-ol … (52, 19)\u003c\/p\u003e \u003cp\u003eMonoalkylation of α,β-Unsaturated Ketones via Metalloenamines: 1-Butyl-10-methyl-Δ\u003csup\u003e1(9)\u003c\/sup\u003e-2-octalone (57, 69)\u003c\/p\u003e \u003cp\u003eβ-Diketones from Methyl Alkyl Ketones: 3-n-Butyl-2,4-pentanedione … (51, 90)\u003c\/p\u003e \u003cp\u003eSecondary and Tertiary Alkyl Ketones from Carboxylic Acid Chlorides and Lithium Phenylthio(alkyl)cuprate Reagents: tert-Butyl Phenyl Ketone … (55, 122)\u003c\/p\u003e \u003cp\u003eRemoval of N\u003csup\u003eα\u003c\/sup\u003e-Benzyloxycarbonyl Groups from Sulfur-Containing Peptides by Catalytic Hydrogenation in Liquid ammonia: O-tert-Butyl-L-seryl-S-tert-butyl-l-cysteine tert-Butyl Ester … (59, 159)\u003c\/p\u003e \u003cp\u003eEsterification of Hindered Alcohols: tert-Butyl p-Toluate … (51, 96)\u003c\/p\u003e \u003cp\u003ePeptide Syntheses Using N-Ethyl-5-phenylisoxazolium-3’-sulfonate:\u003c\/p\u003e \u003cp\u003eCarbobenzoxy-L-asparaginyl-L-leucine Methyl Ester and N-Carbobenzoxy-3-hydroxy-L-prolylglycylglycine Ethyl Ester … (56, 88)\u003c\/p\u003e \u003cp\u003eCarbonyl Cyanide … (51, 70)\u003c\/p\u003e \u003cp\u003e3-Chlorocyclobutanecarboxylic Acid … (51, 73)\u003c\/p\u003e \u003cp\u003e(z)-4-Chloro-4-hexenyl Trifluoroacetate … (57, 26)\u003c\/p\u003e \u003cp\u003em-Chloroperbenzoic Acid … (50, 15)\u003c\/p\u003e \u003cp\u003e3-(4-Chlorophenyl)-5-(4-Methoxyphenyl)Isoxazole … (55, 39)\u003c\/p\u003e \u003cp\u003eα-Chloro Enamines, Reactive Intermediates for Synthesis: 1-Chloro-N,N,2-trimethylpropenylamine … (59, 26)\u003c\/p\u003e \u003cp\u003eModified Clemmensen Reduction: Cholestane … (53, 86)\u003c\/p\u003e \u003cp\u003eConjugate Reduction of α,β-Unsaturated p-Toluenesulfonylhydrazones to Alkenes with Catecholborane: 5β-Cholest-3-ene … (59, 42)\u003c\/p\u003e \u003cp\u003e5β-Cholest-3-Ene-5-Acetaldehyde … (54, 71)\u003c\/p\u003e \u003cp\u003e18-Crown-6 … (57, 30)\u003c\/p\u003e \u003cp\u003eCinnamonitrile … (50, 18)\u003c\/p\u003e \u003cp\u003ePreparation of Cyano Compounds Using Alkylaluminum Intermediates: 1-Cyano-6-methoxy-3,4-Dihydronaphthalene … (52, 96)\u003c\/p\u003e \u003cp\u003eCyclobutadieneiron Tricarbonyl … (50, 21)\u003c\/p\u003e \u003cp\u003eAldehydes from acid Chlorides by Reduction of Ester-mesylates with Sodium Borohydride: Cyclobutanecarboxaldehyde … (51, 11)\u003c\/p\u003e \u003cp\u003eCyclic Ketones from 1,3-Dithiane: Cyclobutanone … (51, 76)\u003c\/p\u003e \u003cp\u003eCyclobutanone from Methylenecyclopropane via Oxaspiropentane … (57, 36)\u003c\/p\u003e \u003cp\u003eCyclobutanone Via Solvolytic Cyclization … (54, 84)\u003c\/p\u003e \u003cp\u003eOne-carbon Ring Expansion of Cycloalkanones to Conjugated Cycloalkenones: 2-Cyclohepten-1-one … (59, 113)\u003c\/p\u003e \u003cp\u003eNitriles from Ketones: Cyclohexanecarbonitrile … (58, 101)\u003c\/p\u003e \u003cp\u003eAldehydes from Olefins: Cyclohexanecarboxaldehyde … (57, 11)\u003c\/p\u003e \u003cp\u003eCatalytic Osmium Tetroxide Oxidation of Olefins: cis-1,2-Cyclohexanediol … (58, 43)\u003c\/p\u003e \u003cp\u003eStereoselective Hydroxylation with Thallium(i) Acetate and Iodine: trans- and cis-1,2-Cyclohexanediols … (59, 169)\u003c\/p\u003e \u003cp\u003eCleavage of Methyl Ethers with Iodotrimethylsilane: Cyclohexanol from Cyclohexyl Methyl Ether … (59, 35)\u003c\/p\u003e \u003cp\u003ePreparation of α,β-Unsaturated Aldehydes via the Wittig Reaction: Cyclohexylideneacetaldehyde … (53, 104)\u003c\/p\u003e \u003cp\u003eCyclopropenone … (57, 41)\u003c\/p\u003e \u003cp\u003eCyclopropyldiphenylsulfonium Tetrafluoroborate … (54, 27)\u003c\/p\u003e \u003cp\u003eRing Contraction via a Favorskii-Type Rearrangement: Cycloundecanone … (56, 107)\u003c\/p\u003e \u003cp\u003eHydrogenation of Aromatic Nuclei: 1-Decalol … (51, 103)\u003c\/p\u003e \u003cp\u003eOxidation with the Chromium Trioxide-Pyridine Complex Prepared in situ: 1-Decanal … (55, 84)\u003c\/p\u003e \u003cp\u003eReduction of Alkyl Halides and Tosylates with Sodium Cyanoborohydride in Hexamethylphosphoric Triamide (HMPA): A. 1-Iododecane to n-Decane B. 1-Dodecyl Tosylate to n-Dodecane … (53, 107)\u003c\/p\u003e \u003cp\u003eDiamantane: Pentacyclo[7.3.1.1\u003csup\u003e4,12\u003c\/sup\u003e.0\u003csup\u003e2,7\u003c\/sup\u003e.0\u003csup\u003e6,11\u003c\/sup\u003e]tetradecane … (53, 30)\u003c\/p\u003e \u003cp\u003eMacrocyclic Diimines: 1,10-dlazacyclöCtadecane … (54, 88)\u003c\/p\u003e \u003cp\u003eDlazoacetophenone … (53, 35)\u003c\/p\u003e \u003cp\u003e2-diazocycloalkanones: 2-diazocyclohexanone … (51, 86)\u003c\/p\u003e \u003cp\u003e2-diazopropane … (50, 27)\u003c\/p\u003e \u003cp\u003eMacrocyclic Polyethers: Dibenzo-18-crown-6 Polyether and Dicyclohexyl-18-crown-6 Polyether … (52, 66)\u003c\/p\u003e \u003cp\u003e1,2-Diaroylcyclopropanes: trans-1,2-Dibenzoylcyclopropane … (52, 33)\u003c\/p\u003e \u003cp\u003eα,???-Dibromodibenzyl Sulfone … (50, 31)\u003c\/p\u003e \u003cp\u003ePhosphine-Nickel Complex Catalyzed Cross-Coupling of Grignard Reagents with Aryl and Alkenyl Halides: 1,2-Dibutylbenzene … (58, 127)\u003c\/p\u003e \u003cp\u003eOxidation with Bis(Salicylidene)ethylenediiminocobalt(II) (Salcomine); 2,6-Di-tert-butyl-p-benzoquinone … (57, 78)\u003c\/p\u003e \u003cp\u003eDiazo Transfer by Means of Phase-transfer Catalysis: Di-tert-Butyl Diazomalonate … (59, 66)\u003c\/p\u003e \u003cp\u003eDi-tert-butyl Dicarbonate … (57, 45)\u003c\/p\u003e \u003cp\u003ecis-3,4-Dichlorocyclobutene … (50, 36)\u003c\/p\u003e \u003cp\u003ecis-Dichloroalkanes from Epoxides: cis-1,2-Dichlorocyclohexane … (58, 64)\u003c\/p\u003e \u003cp\u003e2,3-Dicyanobutadiene as a Reactive Intermediate by in situ Generation from 1,2-Dicyanocyclobutene: 2,3-Dicyano-1,4,4a,9a-tetrahydrofluorene … (58, 67)\u003c\/p\u003e \u003cp\u003eDideuteriodiazomethane … (53, 38)\u003c\/p\u003e \u003cp\u003eDiethylaluminum cyanide … (52, 90)\u003c\/p\u003e \u003cp\u003eDiethylaminosulfur trifluoride … (57, 50)\u003c\/p\u003e \u003cp\u003eDiethyl tert-Butylmalonate … (50, 38)\u003c\/p\u003e \u003cp\u003e2-Trimethylsilyloxy-1,3-butadiene as a Reactive Diene: Diethyl trans-4-Trimethylsilyloxy-4-cyclohexene-1,2-dicarboxylate … (58, 163)\u003c\/p\u003e \u003cp\u003eDiethyl 2-(Cyclohexylamino)vinylphosphonate … (53, 44)\u003c\/p\u003e \u003cp\u003eRadical Anion Arylation: Diethyl Phenylphosphonate … (58, 134)\u003c\/p\u003e \u003cp\u003eDiethyl trans-δ\u003csup\u003e4\u003c\/sup\u003e-Tetrahydrophthalate … (50, 43)\u003c\/p\u003e \u003cp\u003eHomogeneous Catalytic Hydrogenation: Dihydrocarvone … (53, 63)\u003c\/p\u003e \u003cp\u003etrans-1,2-Dihydrophthalic Acid … (50, 50)\u003c\/p\u003e \u003cp\u003e5,6-Dihydro-2H-pyran-2-one and 2H-Pyran-2-One … (56, 49)\u003c\/p\u003e \u003cp\u003e2,4-Dimethoxybenzonitrile … (50, 52)\u003c\/p\u003e \u003cp\u003eBiaryls from Simple Arenes via Organotellurium Intermediates; 4,4’-Dimethoxy-1,1’-Biphenyl … (57, 18)\u003c\/p\u003e \u003cp\u003e6,7-Dimethoxy-3-Isochromanone … (55, 45)\u003c\/p\u003e \u003cp\u003eRegioselective Mannich Condensation with Dimethyl(methylene)ammonium Trifluoroacetate: 1-Dimethylamino-4-methyl-3-pentanone … (59, 153)\u003c\/p\u003e \u003cp\u003eDirected Lithiation of Aromatic Compounds: (2-Dimethylamino-5-methylphenyl)diphenylcarbinol … (53, 56)\u003c\/p\u003e \u003cp\u003eUse of Dipotassium Nitrosodisulfonate (fremy’s Salt): 4,5-Dimethyl-o-Benzoquinone … (52, 88)\u003c\/p\u003e \u003cp\u003e1,2-Dimethylcyclobutenes by Reductive Ring-Contraction of Sulfolanes: cis-7,8-Dimethylbicyclo[4.2.0]oct-7-Ene … (57, 53)\u003c\/p\u003e \u003cp\u003e4,4’-Dimethyl-1,1’-biphenyl … (55, 48)\u003c\/p\u003e \u003cp\u003eN,N-Dimethyl-5β-cholest-3-Ene-5-acetamide … (54, 77)\u003c\/p\u003e \u003cp\u003eConversion of Esters to Amides with Dimethylaluminum Amides: N,N-Dimethylcyclohexanecarboxamide … (59, 49)\u003c\/p\u003e \u003cp\u003e4,4-Dimethyl-2-Cyclohexen-1-one … (53, 48)\u003c\/p\u003e \u003cp\u003eReductive Amination with Sodium Cyanoborohydride: N,N- Dimethylcyclohexylamine … (52, 124)\u003c\/p\u003e \u003cp\u003eN,N-Dimethyldodecylamine Oxide … (50, 56)\u003c\/p\u003e \u003cp\u003eDimethyl Nitrosuccinate … (57, 60)\u003c\/p\u003e \u003cp\u003eDimethyl 2,3-Pentadienedioate … (57, 62)\u003c\/p\u003e \u003cp\u003eAllylically Transposed Amines from Allylic Alcohols; 3,7-Dimethyl-1,6-octadien-3-amine … (58, 4)\u003c\/p\u003e \u003cp\u003eBicyclic Ketones for The Synthesis of Tropinoids: 2α,4α-Dimethyl-8-oxabicyclo[3.2.1]oct-6-en-3-one … (58, 17)\u003c\/p\u003e \u003cp\u003e2,2-Dimethyl-4-Phenylbutyric Acid … (50, 58)\u003c\/p\u003e \u003cp\u003eCyclopentenones from α,α’-Dibromoketones and Enamines: 2,5-Dimethyl-3-phenyl-2-cyclopenten-1-one … (58, 56)\u003c\/p\u003e \u003cp\u003eAlkylations of Aldehydes via Reaction of the Magnesioenamine Salt of an Aldehyde: 2,2-Dimethyl-3-phenylpropionaldehyde … (54, 46)\u003c\/p\u003e \u003cp\u003e3,5-Dinitrobenzaldehyde … (53, 52)\u003c\/p\u003e \u003cp\u003e2,3-Diphenyl-1,3-butadiene … (50, 62)\u003c\/p\u003e \u003cp\u003eReagents for Synthesis of Organoselenium Compounds: Diphenyl Diselenide and Benzeneselenenyl Chloride … (59, 141)\u003c\/p\u003e \u003cp\u003eAromatic Hydrocarbons from Aromatic Ketones and Aldehydes: 1,1-Diphenylethane … (55, 7)\u003c\/p\u003e \u003cp\u003eNucleophilic α-sec-Aminoalkylation: 2-(Diphenylhydroxymethyl)pyrrolidine … (58, 113)\u003c\/p\u003e \u003cp\u003eDiphenylketene … (52, 36)\u003c\/p\u003e \u003cp\u003eAlkenes via Hofmann Elimination: Use of Ion-Exchange Resin for Preparation of Quaternary Ammonium Hydroxides: Diphenylmethyl Vinyl Ether … (55, 3)\u003c\/p\u003e \u003cp\u003e2,3-Diphenylvinylene Sulfone … (50, 65)\u003c\/p\u003e \u003cp\u003e1,3-Dithiane … (50, 72)\u003c\/p\u003e \u003cp\u003e2,2’-Dithienyl Sulfide … (50, 75)\u003c\/p\u003e \u003cp\u003eSelective Epoxidation of Terminal Double Bonds: 10, 11-Epoxyfarnesyl Acetate … (56, 112)\u003c\/p\u003e \u003cp\u003e1-Ethoxy-1-butyne … (57, 65)\u003c\/p\u003e \u003cp\u003eDemethylation of Methyl Aryl Ethers: 4-Ethoxy-3-hydroxybenzaldehyde … (56, 44)\u003c\/p\u003e \u003cp\u003eCarbine Generation by α-Elimination with Lithium 2,2,6,6-Tetramethylpiperidide: 1-Ethoxy-2-p-tolylcyclopropane … (58, 37)\u003c\/p\u003e \u003cp\u003eEsterification of Carboxylic Acids with Trialkyloxonium Salts; Ethyl and Methyl 4-Acetoxybenzoates … (56, 59)\u003c\/p\u003e \u003cp\u003eortho-Alkylation of Anilines: Ethyl 4-Amino-3-Methylbenzoate … (56, 15)\u003c\/p\u003e \u003cp\u003eEthyl 5β-Cholest-3-ene-5-acetate … (54, 74)\u003c\/p\u003e \u003cp\u003eFree-Radical Cyclization: Ethyl 1-Cyano-2-Methylcyclohexanecarboxylate … (55, 57)\u003c\/p\u003e \u003cp\u003e2,2-(Ethylenedithio)cyclohexanone … (54, 37)\u003c\/p\u003e \u003cp\u003eA General Synthesis of 4-Isoxazolecarboxylic Esters: Ethyl 3-Ethyl-5-methyl-4-isoxazolecarboxylate … (53, 59)\u003c\/p\u003e \u003cp\u003e3-Alkyl-1-alkynes Synthesis: 3-Ethyl-1-hexyne … (58, 1)\u003c\/p\u003e \u003cp\u003eβ-Hydroxy Esters from Ethyl Acetate and Aldehydes or Ketones: Ethyl 1-Hydroxycyclohexylacetate … (53, 66)\u003c\/p\u003e \u003cp\u003eIndoles from Anilines: Ethyl 2-Methylindole-5-carboxylate … (56, 72)\u003c\/p\u003e \u003cp\u003eStereoselective Synthesis of Trisubstituted Olefins: Ethyl 4-Methyl-(E)-4,8-nonadienoate … (53, 116)\u003c\/p\u003e \u003cp\u003eMetalation of 2-Methylpyridine Derivatives: Ethyl 6-Methylpyridine-2-acetate … (52, 75)\u003c\/p\u003e \u003cp\u003eEthyl 1-Naphthylacetate … (50, 77)\u003c\/p\u003e \u003cp\u003eEthyl … (E)-3-Nitroacrylate [Replaced by Methyl … (E)-3-Nitroacrylate] … (56, 65; replaced)\u003c\/p\u003e \u003cp\u003eγ-Ketoesters from Aldehydes via Diethyl Acylsuccinates: Ethyl 4-oxohexanoate … (58, 79)\u003c\/p\u003e \u003cp\u003eEthyl Pyrrole-2-Carboxylate … (51, 100)\u003c\/p\u003e \u003cp\u003eThiazoles from Ethyl Isocyanoacetate and Thiono Esters: Ethyl Thiazole-4-carboxylate … (59, 183)\u003c\/p\u003e \u003cp\u003eCarboxylation of Aromatic Compounds: Ferrocenecarboxylic Acid … (56, 28)\u003c\/p\u003e \u003cp\u003eFluorinations with Pyridinium Polyhydrogen Fluoride Reagent: 1-Fluoroadamantane … (58, 75)\u003c\/p\u003e \u003cp\u003eAldehydes from Aromatic Nitriles: 4-Formylbenzenesulfonamide … (51, 20)\u003c\/p\u003e \u003cp\u003eGeranyl Chloride … (54, 63)\u003c\/p\u003e \u003cp\u003eAllylic Chlorides from Allylic Alcohols: Geranyl Chloride … (54, 68)\u003c\/p\u003e \u003cp\u003eGlutaconaldehyde Sodium Salt From Hydrolysis of Pyridinium-1-sulfonate … (59, 79)\u003c\/p\u003e \u003cp\u003eAldehydes from Primary Alcohols by Oxidation with Chromium Trioxide: Heptanal … (52, 5)\u003c\/p\u003e \u003cp\u003eConversion of Nitro to Carbonyl by Ozonolysis of Nitronates: 2,5-Heptanedione … (56, 36)\u003c\/p\u003e \u003cp\u003eMacrocyclic Polyamines: 1,4,7,10,13,16-Hexaäzacycloöctadecane … (58, 86)\u003c\/p\u003e \u003cp\u003eCuprous Ion-Catalyzed Oxidative Cleavage of Aromatic o-Diamines by Oxygen:(Z,Z)-2,4-Hexadienedinitrile … (57, 33)\u003c\/p\u003e \u003cp\u003eHexafluoroacetone Imine … (50, 81)\u003c\/p\u003e \u003cp\u003e3-Trimethylsilyl-3-buten-2-one as Michael Acceptor for Conjugate Addition-Annelation: cis-4,4a,5,6,7,8-Hexahydro-4a,5-dimethyl-2(3H)-naphthalenone … (58, 158)\u003c\/p\u003e \u003cp\u003eNitrones for Intramolecular 1,3-Dipolar Cycloadditions: Hexahydro-1,3,3,6-tetramethyl-2,1-benzisoxazoline … (58, 106)\u003c\/p\u003e \u003cp\u003e(E)-4-Hexen-1-ol … (55, 62)\u003c\/p\u003e \u003cp\u003eFragmentation of α,β-Epoxyketones to Acetylenic Aldehydes and Ketones: Preparation of 2,3-Epoxycyclohexanone and its Fragmentation to 5-Hexynal … (55, 52)\u003c\/p\u003e \u003cp\u003eγ-Hydroxy-α,β-Unsaturated Aldehydes via 1,3-Bis(methylthio)allyllithium: trans-4-Hydroxy-2-hexenal … (54, 19)\u003c\/p\u003e \u003cp\u003e17β-Hydroxy-5-oxo-3,5-seco-4-norandrostane-3-carboxylic Acid … (55, 67)\u003c\/p\u003e \u003cp\u003eDirected Aldol Condensations: threo-4-Hydroxy-3-phenyl-2-heptanone … (54, 49)\u003c\/p\u003e \u003cp\u003eMacrolides from Cyclization of ω-Bromocarboxylic Acids: 11-Hydroxyundecanoic Lactone … (58, 98)\u003c\/p\u003e \u003cp\u003eDirect Iodination of Polyalkylbenzenes: Iododurene … (51, 94)\u003c\/p\u003e \u003cp\u003etrans-Iodopropenylation of Alkyl Halides: (E)-1-Iodo-4-phenyl-2-butene … (56, 77)\u003c\/p\u003e \u003cp\u003e2-Iodo-p-xylene … (55, 70)\u003c\/p\u003e \u003cp\u003ecis-α,β-Unsaturated Acids: Isocrotonic Acid … (53, 123)\u003c\/p\u003e \u003cp\u003eTrichloromethyl Chloroformate as a Phosgene Equivalent: 3-Isocyanatopropanoyl Chloride … (59, 195)\u003c\/p\u003e \u003cp\u003eHydroboration of Olefins: (+)-Isopinocampheol [Replaced by (—)-Isopinocampheol] … (52, 59)\u003c\/p\u003e \u003cp\u003e(—)-Isopinocampheol (New)\u003c\/p\u003e \u003cp\u003eReaction of Aryl Halides with π-Allylnickel Halides: Methallylbenzene … (52, 115)\u003c\/p\u003e \u003cp\u003eSulfonyl Cyanides: Methanesulfonyl Cyanide … (57, 88)\u003c\/p\u003e \u003cp\u003e1,6-Methano[10]annulene … (54, 11)\u003c\/p\u003e \u003cp\u003eVinyl Sulfides from Thioacetals with Copper(I) Trifluoromethanesulfonate: (Z)-2-Methoxy-1-phenylthio-1,3-butadiene … (59, 202)\u003c\/p\u003e \u003cp\u003e6-Methoxy-β-tetralone … (51, 109)\u003c\/p\u003e \u003cp\u003eMethyl Groups by Reduction of Aromatic Carboxylic Acids with Trichlorosilane-tri-n-propylamine: 2-Methylbiphenyl … (56, 83)\u003c\/p\u003e \u003cp\u003e1-d-Aldehydes from Organometallic Reagents: 2-Methylbutanal-1-d … (51, 31)\u003c\/p\u003e \u003cp\u003ePreparation of Vinyl Trifluoromethanesulfonates: 3-methyl-2-buten-2-yl Triflate … (54, 79)\u003c\/p\u003e \u003cp\u003ePreparation and Reductive Cleavage of Enol Phosphates: 5-Methylcoprost-3-Ene … (52, 109)\u003c\/p\u003e \u003cp\u003eOxymercuration-Reduction: Alcohols from Olefins: 1-Methylcyclohexanol … (53, 94)\u003c\/p\u003e \u003cp\u003eReductive Cleavage of Allylic Alcohols, Ethers, or Acetates to Olefins: 3-Methylcyclohexene … (56, 101)\u003c\/p\u003e \u003cp\u003eγ-Ketoesters to Prepare Cyclic Diketones: 2-Methyl-1,3-cyclopentanedione … (58, 83)\u003c\/p\u003e \u003cp\u003eSulfide Contraction via Alkylative Coupling: 3-Methyl-2,4-Heptanedione … (55, 127)\u003c\/p\u003e \u003cp\u003eIsoxazole Annelation Reaction: 1-Methyl-4,4a,5,6,7,8-Hexahydronaphthalen-2(3H)-one … (53, 70)\u003c\/p\u003e \u003cp\u003eAddition of Organolithium Reagents to Allyl Alcohol: 2-Methyl-1-Hexanol … (55, 1)\u003c\/p\u003e \u003cp\u003eConversion of Primary Alcohols to Urethanes via the Inner Salt of Methyl (carboxysulfamoyl)Triethylammonium Hydroxide: Methyl n-Hexylcarbamate … (56, 40)\u003c\/p\u003e \u003cp\u003eMethyl 2-Alkynoates from 3-Alkyl-2-pyrazolin-5-ones: Methyl 2-Hexynoate … (55, 73)\u003c\/p\u003e \u003cp\u003eMethyl (trans-2-Iodo-1-Tetralin)carbamate … (51, 112)\u003c\/p\u003e \u003cp\u003eMethyl Nitroacetate … (55, 77)\u003c\/p\u003e \u003cp\u003eMethyl (E)-3-Nitroacrylate (New)\u003c\/p\u003e \u003cp\u003e2-Methyl-2-nitrosopropane and Its Dimer … (52, 77)\u003c\/p\u003e \u003cp\u003eNucleophilic Acylation with Disodium Tetracarbonylferrate: Methyl 7-Oxoheptanoate and Methyl 7-Oxoöctanoate … (59, 102)\u003c\/p\u003e \u003cp\u003eAldehydes from Allylic Alcohols and Phenylpalladium Acetate: 2-Methyl-3-phenylpropionalde … (51, 17)\u003c\/p\u003e \u003cp\u003eEndocyclic Enamine Synthesis: N-Methyl-2-phenyl-Δ\u003csup\u003e2\u003c\/sup\u003e-tetrahydropyridine … (54, 93)\u003c\/p\u003e \u003cp\u003eHydrogenolysis of Carbon-Halogen Bonds with Chromium(II)-en Perchlorate: Naphthalene from 1-Bromonaphthalene … (52, 62)\u003c\/p\u003e \u003cp\u003eThiophenols from Phenols: 2-Naphthalenethiol … (51, 139)\u003c\/p\u003e \u003cp\u003eS(-)-α-(1-Naphthyl)ethylamine … (55, 80)\u003c\/p\u003e \u003cp\u003eAlkyl Iodides: Neopentyl Iodide and Iodocyclohexane … (51, 44)\u003c\/p\u003e \u003cp\u003eSulfide Synthesis in Preparation of Dialkyl and Alkyl Aryl Sulfides: Neopentyl Phenyl Sulfide (58, 143)\u003c\/p\u003e \u003cp\u003e4-Nitrobenzyl Fluoride … (57, 72)\u003c\/p\u003e \u003cp\u003e1-Nitrocycloöctene … (50, 84)\u003c\/p\u003e \u003cp\u003eFormation and Photochemical Wolff Rearrangement of Cyclic α-Diazo Ketones: D-Norandrost-5-en-3β-ol-16-carboxylic Acids … (52, 53)\u003c\/p\u003e \u003cp\u003eHighly Reactive Magnesium for the Preparation of Griignard Reagents: 1-Norbornanecarboxylic Acid … (59, 85)\u003c\/p\u003e \u003cp\u003eΔ\u003csup\u003e9,10\u003c\/sup\u003e-Octalin … (50, 88)\u003c\/p\u003e \u003cp\u003e 2,2,7,7,12,12,17,17-Octamethyl-21,22,23,24-tetraoxaperhydroquaterene … (57, 74)\u003c\/p\u003e \u003cp\u003eOrcinol Monomethyl Ether … (53, 90)\u003c\/p\u003e \u003cp\u003e1,6-Oxido[10]annulene … (55, 86)\u003c\/p\u003e \u003cp\u003eCyanide-Catalyzed Conjugate Addition of Aryl Aldehydes: 4-Oxo-4-(3-pyridyl)butyronitrile … (59, 53)\u003c\/p\u003e \u003cp\u003eAldehydes from sym-Trithlane: n-Pentadecanal … (51, 39)\u003c\/p\u003e \u003cp\u003e(Pentafluorophenyl)acetonitrile … (57, 80)\u003c\/p\u003e \u003cp\u003ePentafluorophenylcopper Tetramer, a Reagent for Synthesis of Fluorinated Aromatic Compounds … (59, 122)\u003c\/p\u003e \u003cp\u003etrans-3-Penten-2-one … (51, 115)\u003c\/p\u003e \u003cp\u003eArene Oxide Synthesis: Phenanthrene-9,10-oxide … (58, 12)\u003c\/p\u003e \u003cp\u003eFree-Radical Alkylation of Quinones: 2-Phenoxymethyl-1,4-Benzoquinone … (56, 68)\u003c\/p\u003e \u003cp\u003e3-Phenyl-2H-azirine-2-carboxaldehyde … (57, 83)\u003c\/p\u003e \u003cp\u003ePhase-Transfer Alkylation of Nitriles: 2-Phenylbutyronitrile … (55, 91)\u003c\/p\u003e \u003cp\u003eDirected Aldol Condensations: β- Phenylcinnamaldehyde … (50, 66)\u003c\/p\u003e \u003cp\u003eAldehydes from 2-Benzyl-4,4,6-Trimethyl-5,6-dihydro-1,3(4H)-oxazine: 1-Phenylcyclopentanecarboxaldehyde … (51, 24)\u003c\/p\u003e \u003cp\u003eAmines from Mixed Carboxylic-Carbonic Anhydrides: 1-Phenylcyclopentylamine … (51, 48)\u003c\/p\u003e \u003cp\u003ecis-2-Phenylcyclofropanecarboxylic Acid … (50, 94)\u003c\/p\u003e \u003cp\u003eSubstitution of Aryl Halides with Copper(i) Acetylides: 2-Phenylfuro[3,2-b]pyridine … (52, 128)\u003c\/p\u003e \u003cp\u003eKetones and Alcohols from Organoboranes: Phenyl Heptyl Ketone, 1-Hexanol, and 1-Octanol … (53, 77)\u003c\/p\u003e \u003cp\u003e1-Phenyl-1,4-pentadiyne and 1-Phenyl-1,3-pentadiyne … (50, 97)\u003c\/p\u003e \u003cp\u003ePhenylation with Diphenyliodonium Chloride; 1-Phenyl-2,4-pentanedione … (51, 128)\u003c\/p\u003e \u003cp\u003e1-Phenyl-4-phosphorinanone … (53, 98)\u003c\/p\u003e \u003cp\u003e4-Phenyl-1,2,4-triazoline-3,5-dione … (51, 121)\u003c\/p\u003e \u003cp\u003e2-Phenyl-2-vinylbutyronitrile … (55, 99)\u003c\/p\u003e \u003cp\u003eBoranes in Functionalization of Olefins to Amines: 3-Pinanamine … (58, 32)\u003c\/p\u003e \u003cp\u003eAllylic Oxidation with Hydrogen Peroxide-Selenium Dioxide: trans-Pinocarveol … (56, 25)\u003c\/p\u003e \u003cp\u003eBase-Induced Rearrangement of Epoxides to Allylic Alcohols: trans-Pinocarveol … (53, 17)\u003c\/p\u003e \u003cp\u003ePolymeric Carbodiimide. Preparation … (56, 95)\u003c\/p\u003e \u003cp\u003eAlkynes via Phase Transfer—Catalyzed Dehydrohalogenation: Propiolaldehyde Diethyl Acetal … (59, 10)\u003c\/p\u003e \u003cp\u003eRearrangement of Bridgehead Alcohols to Polycyclic Ketones by Fragmentation-Cyclization: 4-Protoadamantanone (Tricyclo[4.3.1.0\u003csup\u003e3.8\u003c\/sup\u003e]Decan-4-One) … (59, 147)\u003c\/p\u003e \u003cp\u003eQuadricyclane … (51, 133)\u003c\/p\u003e \u003cp\u003e1,2,3,4-Tetrahydro-β-Carboline … (51, 136)\u003c\/p\u003e \u003cp\u003eAziridines from β-Iodocarbamates: 1,2,3,4-Tetrahydronaphthalene(1,2)Imine (51, 53)\u003c\/p\u003e \u003cp\u003e2,3,4,5-Tetrahydropyridine Trimer … (56, 118)\u003c\/p\u003e \u003cp\u003e3,3,6,6-Tetramethoxy-1,4-Cyclohexadiene … (57, 92)\u003c\/p\u003e \u003cp\u003e2,2,3,3-Tetramethyliodocyclopropane … (52, 132)\u003c\/p\u003e \u003cp\u003e4H-1,4-Thiazine l,1-Dioxide … (52, 135)\u003c\/p\u003e \u003cp\u003e2-Thiophenethiol … (50, 104)\u003c\/p\u003e \u003cp\u003ep-Tolylsulfonyldiazomethane … (57, 95)\u003c\/p\u003e \u003cp\u003ep-Tolylsulfonylmethyl Isocyanide … (57, 102)\u003c\/p\u003e \u003cp\u003eTri-tert-Butylcyclopropenyl Tetrafluoroborate … (54, 97)\u003c\/p\u003e \u003cp\u003eTricarbonyl[2,3,4,5-η)-2,4,-Cyclohexadien-1-One]Iron and Tricarbonyl[(1,2,3,4,5-η)-2-Methyoxy-2,4-Cyclohexadien-1-Yl]Iron(1+) Hexafluorophosphate(1—) from Anisole … (57, 107)\u003c\/p\u003e \u003cp\u003eAlkylation of Dimedone with a Tricarbonyl(diene)Iron Complex: Tricarbonyl[2-[2,3,4,5-η)-4-Methoxy-2,4-Cyclohexadien-1-yl]-5,5-Dimethyl-1,3-Cyclohexanedione]iron … (57, 16)\u003c\/p\u003e \u003cp\u003eCyclobutadiene in Synthesis: endo-Tricyclo[4.4.0.0\u003csup\u003e2,5\u003c\/sup\u003e]Deca-3,8-Diene-7,10-Dione … (55, 43)\u003c\/p\u003e \u003cp\u003eTrifluoroacetylation of Amines and Amino Acids Under Neutral, Mild Conditions: N-Trifluoroacetanilide and N-Trifluoroacetyl-L-Tyrosine … (56, 122)\u003c\/p\u003e \u003cp\u003eAldehydes from Acid Chlorides by Modified Rosenmund Reduction: 3,4,5-Trimethoxybenzaldehyde … (51, 8)\u003c\/p\u003e \u003cp\u003eOxidation with the Nitrosodisulfonate Radical. I. Preparation and Use of Disodium Nitrosodisulfonate: Trimethyl-p-Benzoquinone … (52, 83)\u003c\/p\u003e \u003cp\u003e2,2-(Trimethylenedithio)Cyclohexanone … (54, 39)\u003c\/p\u003e \u003cp\u003eTrimethylene Dithiotosylate and Ethylene Dithiotosylate … (54, 33)\u003c\/p\u003e \u003cp\u003eTrimethyloxonium Tetrafluoroborate … (51, 142)\u003c\/p\u003e \u003cp\u003e3,5,5-Trimethyl-2-(2-Oxopropyl)-2-Cyclohexen-1-One … (57, 113)\u003c\/p\u003e \u003cp\u003eAldehydes by Oxidation of Terminal Olefins with Chromyl Chloride: 2,4,4-Trimethylpentanal … (51, 4)\u003c\/p\u003e \u003cp\u003eTrimethylsilyl Azide … (50, 107)\u003c\/p\u003e \u003cp\u003e3-Trimethylsilyl-3-Buten-2-One: a Michael Acceptor … (58, 152)\u003c\/p\u003e \u003cp\u003eTropolone … (57, 117)\u003c\/p\u003e \u003cp\u003ePreparation of Alkenes by Reaction of Lithium Dipropenylcuprates with Alkyl Halides: (E)-2-Undecene … (55, 103; deleted)\u003c\/p\u003e \u003cp\u003eGeneral Index\u003c\/p\u003e \u003cp\u003eFrmula Index\u003c\/p\u003e \u003cp\u003eHazard Index\u003c\/p\u003e \u003cp\u003eAuthor Index\u003c\/p\u003e \u003cp\u003eConcordance Index\u003c\/p\u003e\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003eSubject Areas: Chemistry [\u003ca title=\"See our other books on Chemistry\" href=\"https:\/\/freshlyprintedbooks.co.uk\/search?q=%22Chemistry%20%5BPN%5D%22\"\u003ePN\u003c\/a\u003e]\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\r\n\u003c\/font\u003e","brand":"Wiley","offers":[{"title":"Brand New","offer_id":52298062692632,"sku":"9780471852438","price":173.19,"currency_code":"GBP","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0730\/2037\/5320\/files\/9780471852438.jpg?v=1781733785","url":"https:\/\/freshlyprintedbooks.co.uk\/products\/organic-syntheses-collective-volume-6-hardback-9780471852438","provider":"Freshly Printed Books","version":"1.0","type":"link"}