{"product_id":"handbook-of-green-analytical-chemistry-hardback-9780470972014","title":"Handbook of Green Analytical Chemistry (Hardback) 9780470972014","description":"\u003cfont face=\"Georgia\"\u003e\r\n\u003cp\u003e\u003cfont size=\"6\"\u003eHandbook of Green Analytical Chemistry\u003c\/font\u003e\u003cbr\u003e\r\n\r\n\r\n\r\n\r\n\r\n\u003c\/p\u003e\n\u003cp\u003e\u003cfont size=\"4\"\u003eMiguel de la Guardia (Edited by), M de la Guardia (Author), Salvador Garrigues (Edited by)\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e9780470972014, Wiley\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003eHardback, published 30 March 2012\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e568 pages\u003cbr\u003e24.8 x 19.5 x 3.1 cm, 1.148 kg\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\r\n\r\n\u003cp align=\"justify\"\u003e\u003cem\u003e\u003cfont size=\"3\"\u003e\u003cp\u003e“In conclusion, this is an interesting book for a reader who wants to expand their views on the topic, being edited by two of the most prolific contributors in the field, and carrying contributions from worldwide renowned groups on the subject. All aspects of the analytical process are covered, from sampling to waste management, while keeping an eye on the practical deployment of the method.”  (\u003ci\u003eGreen Processing and Synthesis\u003c\/i\u003e, 1 August 2012)\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e\u003c\/font\u003e\u003c\/em\u003e\u003c\/p\u003e\r\n\r\n\u003cp align=\"justify\"\u003e\u003cstrong\u003e\u003cfont size=\"3\"\u003e\u003cp\u003eThe emerging field of green analytical chemistry is concerned with the development of analytical procedures that minimize consumption of hazardous reagents and solvents, and maximize safety for operators and the environment.  In recent years there have been significant developments in methodological and technological tools to prevent and reduce the deleterious effects of analytical activities; key strategies include recycling, replacement, reduction and detoxification of reagents and solvents.\u003c\/p\u003e \u003cp\u003eThe \u003ci\u003eHandbook of Green Analytical Chemistry\u003c\/i\u003e provides a comprehensive overview of the present state and recent developments in green chemical analysis. A series of detailed chapters, written by international specialists in the field, discuss the fundamental principles of green analytical chemistry and present a catalogue of tools for developing environmentally friendly analytical techniques.\u003c\/p\u003e \u003cp\u003eTopics covered include:\u003c\/p\u003e \u003cul\u003e \u003cli\u003e\n\u003cb\u003eConcepts:\u003c\/b\u003e Fundamental principles, education, laboratory experiments and publication in green analytical chemistry.\u003c\/li\u003e \u003cli\u003e\n\u003cb\u003eThe Analytical Process:\u003c\/b\u003e Green sampling techniques and sample preparation, direct analysis of samples, green methods for capillary electrophoresis, chromatography, atomic spectroscopy, solid phase molecular spectroscopy, derivative molecular spectroscopy and electroanalytical methods.\u003c\/li\u003e \u003cli\u003e\n\u003cb\u003eStrategies:\u003c\/b\u003e Energy saving, automation, miniaturization and photocatalytic treatment of laboratory wastes.\u003c\/li\u003e \u003cli\u003e\n\u003cb\u003eFields of Application:\u003c\/b\u003e Green bioanalytical chemistry, biodiagnostics, environmental analysis and industrial analysis.\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003eThis advanced handbook is a practical resource for experienced analytical chemists who are interested in implementing green approaches in their work.\u003c\/p\u003e\u003c\/font\u003e\u003c\/strong\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e\u003ci\u003eList of Contributors\u003c\/i\u003e xv  \u003cp\u003e\u003ci\u003ePreface\u003c\/i\u003e xix\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSection I: Concepts 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 The Concept of Green Analytical Chemistry 3\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMiguel de la Guardia and Salvador Garrigues\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e1.1 Green Analytical Chemistry in the frame of Green Chemistry 3\u003c\/p\u003e \u003cp\u003e1.2 Green Analytical Chemistry versus Analytical Chemistry 7\u003c\/p\u003e \u003cp\u003e1.3 The ethical compromise of sustainability 9\u003c\/p\u003e \u003cp\u003e1.4 The business opportunities of clean methods 11\u003c\/p\u003e \u003cp\u003e1.5 The attitudes of the scientific community 12\u003c\/p\u003e \u003cp\u003eReferences 14\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Education in Green Analytical Chemistry 17\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMiguel de la Guardia and Salvador Garrigues\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e2.1 The structure of the Analytical Chemistry paradigm 17\u003c\/p\u003e \u003cp\u003e2.2 The social perception of Analytical Chemistry 20\u003c\/p\u003e \u003cp\u003e2.3 Teaching Analytical Chemistry 21\u003c\/p\u003e \u003cp\u003e2.4 Teaching Green Analytical Chemistry 25\u003c\/p\u003e \u003cp\u003e2.5 From the bench to the real world 26\u003c\/p\u003e \u003cp\u003e2.6 Making sustainable professionals for the future 28\u003c\/p\u003e \u003cp\u003eReferences 29\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 Green Analytical Laboratory Experiments 31\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eSuparna Dutta and Arabinda K. Das\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e3.1 Greening the university laboratories 31\u003c\/p\u003e \u003cp\u003e3.2 Green laboratory experiments 33\u003c\/p\u003e \u003cp\u003e3.2.1 Green methods for sample pretreatment 33\u003c\/p\u003e \u003cp\u003e3.2.2 Green separation using liquid-liquid, solid-phase and solventless extractions 37\u003c\/p\u003e \u003cp\u003e3.2.3 Green alternatives for chemical reactions 42\u003c\/p\u003e \u003cp\u003e3.2.4 Green spectroscopy 45\u003c\/p\u003e \u003cp\u003e3.3 The place of Green Analytical Chemistry in the future of our laboratories 52\u003c\/p\u003e \u003cp\u003eReferences 52\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Publishing in Green Analytical Chemistry 55\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eSalvador Garrigues and Miguel de la Guardia\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e4.1 A bibliometric study of the literature in Green Analytical Chemistry 56\u003c\/p\u003e \u003cp\u003e4.2 Milestones of the literature on Green Analytical Chemistry 57\u003c\/p\u003e \u003cp\u003e4.3 The need for powerful keywords 61\u003c\/p\u003e \u003cp\u003e4.4 A new attitude of authors faced with green parameters 62\u003c\/p\u003e \u003cp\u003e4.5 A proposal for editors and reviewers 64\u003c\/p\u003e \u003cp\u003e4.6 The future starts now 65\u003c\/p\u003e \u003cp\u003eReferences 66\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSection II: The Analytical Process 67\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Greening Sampling Techniques 69\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJosé Luis Gómez Ariza and Tamara García Barrera\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e5.1 Greening analytical chemistry solutions for sampling 70\u003c\/p\u003e \u003cp\u003e5.2 New green approaches to reduce problems related to sample losses, sample contamination, transport and storage 70\u003c\/p\u003e \u003cp\u003e5.2.1 Methods based on flow-through solid phase spectroscopy 70\u003c\/p\u003e \u003cp\u003e5.2.2 Methods based on hollow-fiber GC\/HPLC\/CE 71\u003c\/p\u003e \u003cp\u003e5.2.3 Methods based on the use of nanoparticles 75\u003c\/p\u003e \u003cp\u003e5.3 Greening analytical in-line systems 76\u003c\/p\u003e \u003cp\u003e5.4 In-field sampling 77\u003c\/p\u003e \u003cp\u003e5.5 Environmentally friendly sample stabilization 79\u003c\/p\u003e \u003cp\u003e5.6 Sampling for automatization 79\u003c\/p\u003e \u003cp\u003e5.7 Future possibilities in green sampling 80\u003c\/p\u003e \u003cp\u003eReferences 80\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Direct Analysis of Samples 85\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eSergio Armenta and Miguel de la Guardia\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e6.1 Remote environmental sensing 85\u003c\/p\u003e \u003cp\u003e6.1.1 Synthetic Aperture Radar (SAR) images (satellite sensors) 86\u003c\/p\u003e \u003cp\u003e6.1.2 Open-path spectroscopy 86\u003c\/p\u003e \u003cp\u003e6.1.3 Field-portable analyzers 90\u003c\/p\u003e \u003cp\u003e6.2 Process monitoring: in-line, on-line and at-line measurements 91\u003c\/p\u003e \u003cp\u003e6.2.1 NIR spectroscopy 92\u003c\/p\u003e \u003cp\u003e6.2.2 Raman spectroscopy 92\u003c\/p\u003e \u003cp\u003e6.2.3 MIR spectroscopy 93\u003c\/p\u003e \u003cp\u003e6.2.4 Imaging technology and image analysis 93\u003c\/p\u003e \u003cp\u003e6.3 At-line non-destructive or quasi non-destructive measurements 94\u003c\/p\u003e \u003cp\u003e6.3.1 Photoacoustic Spectroscopy (PAS) 94\u003c\/p\u003e \u003cp\u003e6.3.2 Ambient Mass Spectrometry (MS) 95\u003c\/p\u003e \u003cp\u003e6.3.3 Solid sampling plasma sources 95\u003c\/p\u003e \u003cp\u003e6.3.4 Nuclear Magnetic Resonance (NMR) 96\u003c\/p\u003e \u003cp\u003e6.3.5 X-ray spectroscopy 96\u003c\/p\u003e \u003cp\u003e6.3.6 Other surface analysis techniques 97\u003c\/p\u003e \u003cp\u003e6.4 New challenges in direct analysis 97\u003c\/p\u003e \u003cp\u003eReferences 98\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Green Analytical Chemistry Approaches in Sample Preparation 103\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMarek Tobiszewski, Agata Mechlinska and Jacek Namiesnik\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e7.1 About sample preparation 103\u003c\/p\u003e \u003cp\u003e7.2 Miniaturized extraction techniques 104\u003c\/p\u003e \u003cp\u003e7.2.1 Solid-phase extraction (SPE) 104\u003c\/p\u003e \u003cp\u003e7.2.2 Solid-phase microextraction (SPME) 105\u003c\/p\u003e \u003cp\u003e7.2.3 Stir-bar sorptive extraction (SBSE) 106\u003c\/p\u003e \u003cp\u003e7.2.4 Liquid-liquid microextraction 106\u003c\/p\u003e \u003cp\u003e7.2.5 Membrane extraction 108\u003c\/p\u003e \u003cp\u003e7.2.6 Gas extraction 109\u003c\/p\u003e \u003cp\u003e7.3 Alternative solvents 113\u003c\/p\u003e \u003cp\u003e7.3.1 Analytical applications of ionic liquids 113\u003c\/p\u003e \u003cp\u003e7.3.2 Supercritical fluid extraction 114\u003c\/p\u003e \u003cp\u003e7.3.3 Subcritical water extraction 115\u003c\/p\u003e \u003cp\u003e7.3.4 Fluorous phases 116\u003c\/p\u003e \u003cp\u003e7.4 Assisted extractions 117\u003c\/p\u003e \u003cp\u003e7.4.1 Microwave-assisted extraction 117\u003c\/p\u003e \u003cp\u003e7.4.2 Ultrasound-assisted extraction 117\u003c\/p\u003e \u003cp\u003e7.4.3 Pressurized liquid extraction 118\u003c\/p\u003e \u003cp\u003e7.5 Final remarks 119\u003c\/p\u003e \u003cp\u003eReferences 119\u003c\/p\u003e \u003cp\u003e\u003cb\u003e8 Green Sample Preparation with Non-Chromatographic Separation Techniques 125\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMaría Dolores Luque de Castro and Miguel Alcaide Molina\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e8.1 Sample preparation in the frame of the analytical process 125\u003c\/p\u003e \u003cp\u003e8.2 Separation techniques involving a gas–liquid interface 127\u003c\/p\u003e \u003cp\u003e8.2.1 Gas diffusion 127\u003c\/p\u003e \u003cp\u003e8.2.2 Pervaporation 127\u003c\/p\u003e \u003cp\u003e8.2.3 Membrane extraction with a sorbent interface 130\u003c\/p\u003e \u003cp\u003e8.2.4 Distillation and microdistillation 131\u003c\/p\u003e \u003cp\u003e8.2.5 Head-space separation 131\u003c\/p\u003e \u003cp\u003e8.2.6 Hydride generation and cold-mercury vapour formation 133\u003c\/p\u003e \u003cp\u003e8.3 Techniques involving a liquid–liquid interface 133\u003c\/p\u003e \u003cp\u003e8.3.1 Dialysis and microdialysis 133\u003c\/p\u003e \u003cp\u003e8.3.2 Liquid–liquid extraction 134\u003c\/p\u003e \u003cp\u003e8.3.3 Single-drop microextraction 137\u003c\/p\u003e \u003cp\u003e8.4 Techniques involving a liquid–solid interface 139\u003c\/p\u003e \u003cp\u003e8.4.1 Solid-phase extraction 139\u003c\/p\u003e \u003cp\u003e8.4.2 Solid-phase microextraction 141\u003c\/p\u003e \u003cp\u003e8.4.3 Stir-bar sorptive extraction 142\u003c\/p\u003e \u003cp\u003e8.4.4 Continuous filtration 143\u003c\/p\u003e \u003cp\u003e8.5 A Green future for sample preparation 145\u003c\/p\u003e \u003cp\u003eReferences 145\u003c\/p\u003e \u003cp\u003e\u003cb\u003e9 Capillary Electrophoresis 153\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMihkel Kaljurand\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e9.1 The capillary electrophoresis separation techniques 153\u003c\/p\u003e \u003cp\u003e9.2 Capillary electrophoresis among other liquid phase separation methods 155\u003c\/p\u003e \u003cp\u003e9.2.1 Basic instrumentation for liquid phase separations 155\u003c\/p\u003e \u003cp\u003e9.2.2 CE versus HPLC from the point of view of Green Analytical Chemistry 156\u003c\/p\u003e \u003cp\u003e9.2.3 CE as a method of choice for portable instruments 159\u003c\/p\u003e \u003cp\u003e9.2.4 World-to-chip interfacing and the quest for a ‘killer’ application for LOC devices 163\u003c\/p\u003e \u003cp\u003e9.2.5 Gradient elution moving boundary electrophoresis and electrophoretic exclusion 165\u003c\/p\u003e \u003cp\u003e9.3 Possible ways of surmounting the disadvantages of CE 167\u003c\/p\u003e \u003cp\u003e9.4 Sample preparation in CE 168\u003c\/p\u003e \u003cp\u003e9.5 Is capillary electrophoresis a green alternative? 169\u003c\/p\u003e \u003cp\u003eReferences 170\u003c\/p\u003e \u003cp\u003e\u003cb\u003e10 Green Chromatography 175\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eChi-Yu Lu\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e10.1 Greening liquid chromatography 175\u003c\/p\u003e \u003cp\u003e10.2 Green solvents 176\u003c\/p\u003e \u003cp\u003e10.2.1 Hydrophilic solvents 176\u003c\/p\u003e \u003cp\u003e10.2.2 Ionic liquids 177\u003c\/p\u003e \u003cp\u003e10.2.3 Supercritical Fluid Chromatography (SFC) 177\u003c\/p\u003e \u003cp\u003e10.3 Green instruments 178\u003c\/p\u003e \u003cp\u003e10.3.1 Microbore Liquid Chromatography (microbore LC) 179\u003c\/p\u003e \u003cp\u003e10.3.2 Capillary Liquid Chromatography (capillary LC) 180\u003c\/p\u003e \u003cp\u003e10.3.3 Nano Liquid Chromatography (nano LC) 181\u003c\/p\u003e \u003cp\u003e10.3.4 How to transfer the LC condition from traditional LC to microbore LC, capillary LC or nano LC 182\u003c\/p\u003e \u003cp\u003e10.3.5 Homemade micro-scale analytical system 183\u003c\/p\u003e \u003cp\u003e10.3.6 Ultra Performance Liquid Chromatography (UPLC) 184\u003c\/p\u003e \u003cp\u003eReferences 185\u003c\/p\u003e \u003cp\u003e\u003cb\u003e11 Green Analytical Atomic Spectrometry 199\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMartín Resano, Esperanza García-Ruiz and Miguel A. Belarra\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e11.1 Atomic spectrometry in the context of Green Analytical Chemistry 199\u003c\/p\u003e \u003cp\u003e11.2 Improvements in sample pretreatment strategies 202\u003c\/p\u003e \u003cp\u003e11.2.1 Specific improvements 202\u003c\/p\u003e \u003cp\u003e11.2.2 Slurry methods 204\u003c\/p\u003e \u003cp\u003e11.3 Direct solid sampling techniques 205\u003c\/p\u003e \u003cp\u003e11.3.1 Basic operating principles of the techniques discussed 205\u003c\/p\u003e \u003cp\u003e11.3.2 Sample requirements and pretreatment strategies 207\u003c\/p\u003e \u003cp\u003e11.3.3 Analyte monitoring: The arrival of high-resolution continuum source atomic absorption spectrometry 208\u003c\/p\u003e \u003cp\u003e11.3.4 Calibration 210\u003c\/p\u003e \u003cp\u003e11.3.5 Selected applications 210\u003c\/p\u003e \u003cp\u003e11.4 Future for green analytical atomic spectrometry 213\u003c\/p\u003e \u003cp\u003eReferences 215\u003c\/p\u003e \u003cp\u003e\u003cb\u003e12 Solid Phase Molecular Spectroscopy 221\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eAntonio Molina-Díaz, Juan Francisco García-Reyes and Natividad Ramos-Martos\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e12.1 Solid phase molecular spectroscopy: an approach to Green Analytical Chemistry 221\u003c\/p\u003e \u003cp\u003e12.2 Fundamentals of solid phase molecular spectroscopy 222\u003c\/p\u003e \u003cp\u003e12.2.1 Solid phase absorption (spectrophotometric) procedures 222\u003c\/p\u003e \u003cp\u003e12.2.2 Solid phase emission (fluorescence) procedures 225\u003c\/p\u003e \u003cp\u003e12.3 Batch mode procedures 225\u003c\/p\u003e \u003cp\u003e12.4 Flow mode procedures 226\u003c\/p\u003e \u003cp\u003e12.4.1 Monitoring an intrinsic property 227\u003c\/p\u003e \u003cp\u003e12.4.2 Monitoring derivative species 231\u003c\/p\u003e \u003cp\u003e12.4.3 Recent flow-SPMS based approaches 232\u003c\/p\u003e \u003cp\u003e12.5 Selected examples of application of solid phase molecular spectroscopy 233\u003c\/p\u003e \u003cp\u003e12.6 The potential of flow solid phase envisaged from the point of view of Green Analytical Chemistry 235\u003c\/p\u003e \u003cp\u003eReferences 240\u003c\/p\u003e \u003cp\u003e\u003cb\u003e13 Derivative Techniques in Molecular Absorption, Fluorimetry and Liquid Chromatography as Tools for Green Analytical Chemistry 245\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJosé Manuel Cano Pavón, Amparo García de Torres, Catalina Bosch Ojeda, Fuensanta Sánchez Rojas and Elisa I. Vereda Alonso\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e13.1 The derivative technique as a tool for Green Analytical Chemistry 245\u003c\/p\u003e \u003cp\u003e13.1.1 Theoretical aspects 246\u003c\/p\u003e \u003cp\u003e13.2 Derivative absorption spectrometry in the UV-visible region 247\u003c\/p\u003e \u003cp\u003e13.2.1 Strategies to greener derivative spectrophotometry 248\u003c\/p\u003e \u003cp\u003e13.3 Derivative fluorescence spectrometry 250\u003c\/p\u003e \u003cp\u003e13.3.1 Derivative synchronous fluorescence spectrometry 251\u003c\/p\u003e \u003cp\u003e13.4 Use of derivative signal techniques in liquid chromatography 254\u003c\/p\u003e \u003cp\u003eReferences 255\u003c\/p\u003e \u003cp\u003e\u003cb\u003e14 Greening Electroanalytical Methods 261\u003cbr\u003e \u003c\/b\u003e\u003ci\u003ePaloma Yáñez-Sedeño, José M. Pingarrón and Lucas Hernández\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e14.1 Towards a more environmentally friendly electroanalysis 261\u003c\/p\u003e \u003cp\u003e14.2 Electrode materials 262\u003c\/p\u003e \u003cp\u003e14.2.1 Alternatives to mercury electrodes 262\u003c\/p\u003e \u003cp\u003e14.2.2 Nanomaterial-based electrodes 268\u003c\/p\u003e \u003cp\u003e14.3 Solvents 270\u003c\/p\u003e \u003cp\u003e14.3.1 Ionic liquids 271\u003c\/p\u003e \u003cp\u003e14.3.2 Supercritical fluids 273\u003c\/p\u003e \u003cp\u003e14.4 Electrochemical detection in flowing solutions 274\u003c\/p\u003e \u003cp\u003e14.4.1 Injection techniques 274\u003c\/p\u003e \u003cp\u003e14.4.2 Miniaturized systems 276\u003c\/p\u003e \u003cp\u003e14.5 Biosensors 278\u003c\/p\u003e \u003cp\u003e14.5.1 Greening biosurface preparation 278\u003c\/p\u003e \u003cp\u003e14.5.2 Direct electrochemical transfer of proteins 281\u003c\/p\u003e \u003cp\u003e14.6 Future trends in green electroanalysis 282\u003c\/p\u003e \u003cp\u003eReferences 282\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSection III: Strategies 289\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e15 Energy Savings in Analytical Chemistry 291\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMihkel Koel\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e15.1 Energy consumption in analytical methods 291\u003c\/p\u003e \u003cp\u003e15.2 Economy and saving energy in laboratory practice 294\u003c\/p\u003e \u003cp\u003e15.2.1 Good housekeeping, control and maintenance 295\u003c\/p\u003e \u003cp\u003e15.3 Alternative sources of energy for processes 296\u003c\/p\u003e \u003cp\u003e15.3.1 Using microwaves in place of thermal heating 297\u003c\/p\u003e \u003cp\u003e15.3.2 Using ultrasound in sample treatment 299\u003c\/p\u003e \u003cp\u003e15.3.3 Light as a source of energy 301\u003c\/p\u003e \u003cp\u003e15.4 Using alternative solvents for energy savings 302\u003c\/p\u003e \u003cp\u003e15.4.1 Advantages of ionic liquids 303\u003c\/p\u003e \u003cp\u003e15.4.2 Using subcritical and supercritical fluids 303\u003c\/p\u003e \u003cp\u003e15.5 Efficient laboratory equipment 305\u003c\/p\u003e \u003cp\u003e15.5.1 Trends in sample treatment 306\u003c\/p\u003e \u003cp\u003e15.6 Effects of automation and micronization on energy consumption 307\u003c\/p\u003e \u003cp\u003e15.6.1 Miniaturization in sample treatment 308\u003c\/p\u003e \u003cp\u003e15.6.2 Using sensors 310\u003c\/p\u003e \u003cp\u003e15.7 Assessment of energy efficiency 312\u003c\/p\u003e \u003cp\u003eReferences 316\u003c\/p\u003e \u003cp\u003e\u003cb\u003e16 Green Analytical Chemistry and Flow Injection Methodologies 321\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eLuis Dante Martínez, Soledad Cerutti and Raúl Andrés Gil\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e16.1 Progress of automated techniques for Green Analytical Chemistry 321\u003c\/p\u003e \u003cp\u003e16.2 Flow injection analysis 322\u003c\/p\u003e \u003cp\u003e16.3 Sequential injection analysis 325\u003c\/p\u003e \u003cp\u003e16.4 Lab-on-valve 327\u003c\/p\u003e \u003cp\u003e16.5 Multicommutation 328\u003c\/p\u003e \u003cp\u003e16.6 Conclusions and remarks 334\u003c\/p\u003e \u003cp\u003eReferences 334\u003c\/p\u003e \u003cp\u003e\u003cb\u003e17 Miniaturization 339\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eAlberto Escarpa, Miguel Ángel López and Lourdes Ramos\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e17.1 Current needs and pitfalls in sample preparation 340\u003c\/p\u003e \u003cp\u003e17.2 Non-integrated approaches for miniaturized sample preparation 341\u003c\/p\u003e \u003cp\u003e17.2.1 Gaseous and liquid samples 341\u003c\/p\u003e \u003cp\u003e17.2.2 Solid samples 350\u003c\/p\u003e \u003cp\u003e17.3 Integrated approaches for sample preparation on microfluidic platforms 353\u003c\/p\u003e \u003cp\u003e17.3.1 Microfluidic platforms in sample preparation process 353\u003c\/p\u003e \u003cp\u003e17.3.2 The isolation of analyte from the sample matrix: filtering approaches 356\u003c\/p\u003e \u003cp\u003e17.3.3 The isolation of analytes from the sample matrix: extraction approaches 360\u003c\/p\u003e \u003cp\u003e17.3.4 Preconcentration approaches using electrokinetics 365\u003c\/p\u003e \u003cp\u003e17.3.5 Derivatization schemes on microfluidic platforms 372\u003c\/p\u003e \u003cp\u003e17.3.6 Sample preparation in cell analysis 373\u003c\/p\u003e \u003cp\u003e17.4 Final remarks 378\u003c\/p\u003e \u003cp\u003eReferences 379\u003c\/p\u003e \u003cp\u003e\u003cb\u003e18 Micro- and Nanomaterials Based Detection Systems Applied in Lab-on-a-Chip Technology 389\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMariana Medina-Sánchez and Arben Merkoçi\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e18.1 Micro- and nanotechnology in Green Analytical Chemistry 389\u003c\/p\u003e \u003cp\u003e18.2 Nanomaterials-based (bio)sensors 390\u003c\/p\u003e \u003cp\u003e18.2.1 Optical nano(bio)sensors 391\u003c\/p\u003e \u003cp\u003e18.2.2 Electrochemical nano(bio)sensors 393\u003c\/p\u003e \u003cp\u003e18.2.3 Other detection principles 395\u003c\/p\u003e \u003cp\u003e18.3 Lab-on-a-chip (LOC) technology 396\u003c\/p\u003e \u003cp\u003e18.3.1 Miniaturization and nano-\/microfluidics 396\u003c\/p\u003e \u003cp\u003e18.3.2 Micro- and nanofabrication techniques 397\u003c\/p\u003e \u003cp\u003e18.4 LOC applications 398\u003c\/p\u003e \u003cp\u003e18.4.1 LOCs with optical detections 398\u003c\/p\u003e \u003cp\u003e18.4.2 LOCs with electrochemical detectors 398\u003c\/p\u003e \u003cp\u003e18.4.3 LOCs with other detections 399\u003c\/p\u003e \u003cp\u003e18.5 Conclusions and future perspectives 400\u003c\/p\u003e \u003cp\u003eReferences 401\u003c\/p\u003e \u003cp\u003e\u003cb\u003e19 Photocatalytic Treatment of Laboratory Wastes Containing Hazardous Organic Compounds 407\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eEdmondo Pramauro, Alessandra Bianco Prevot and Debora Fabbri\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e19.1 Photocatalysis 407\u003c\/p\u003e \u003cp\u003e19.2 Fundamentals of the photocatalytic process 408\u003c\/p\u003e \u003cp\u003e19.3 Limits of the photocatalytic treatment 408\u003c\/p\u003e \u003cp\u003e19.4 Usual photocatalytic procedure in laboratory practice 408\u003c\/p\u003e \u003cp\u003e19.4.1 Solar detoxification of laboratory waste 409\u003c\/p\u003e \u003cp\u003e19.5 Influence of experimental parameters 411\u003c\/p\u003e \u003cp\u003e19.5.1 Dissolved oxygen 411\u003c\/p\u003e \u003cp\u003e19.5.2 pH 411\u003c\/p\u003e \u003cp\u003e19.5.3 Catalyst concentration 412\u003c\/p\u003e \u003cp\u003e19.5.4 Degradation kinetics 412\u003c\/p\u003e \u003cp\u003e19.6 Additives reducing the e−\/h+ recombination 412\u003c\/p\u003e \u003cp\u003e19.7 Analytical control of the photocatalytic treatment 413\u003c\/p\u003e \u003cp\u003e19.8 Examples of possible applications of photocatalysis to the treatment of laboratory wastes 413\u003c\/p\u003e \u003cp\u003e19.8.1 Percolates containing soluble aromatic contaminants 414\u003c\/p\u003e \u003cp\u003e19.8.2 Photocatalytic destruction of aromatic amine residues in aqueous wastes 414\u003c\/p\u003e \u003cp\u003e19.8.3 Degradation of aqueous wastes containing pesticides residue 415\u003c\/p\u003e \u003cp\u003e19.8.4 The peculiar behaviour of triazine herbicides 416\u003c\/p\u003e \u003cp\u003e19.8.5 Treatment of aqueous wastes containing organic solvent residues 416\u003c\/p\u003e \u003cp\u003e19.8.6 Treatment of surfactant-containing aqueous wastes 416\u003c\/p\u003e \u003cp\u003e19.8.7 Degradation of aqueous solutions of azo-dyes 419\u003c\/p\u003e \u003cp\u003e19.8.8 Treatment of laboratory waste containing pharmaceuticals 419\u003c\/p\u003e \u003cp\u003e19.9 Continuous monitoring of photocatalytic treatment 420\u003c\/p\u003e \u003cp\u003eReferences 420\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSection IV: Fields of Application 425\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e20 Green Bioanalytical Chemistry 427\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eTadashi Nishio and Hideko Kanazawa\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e20.1 The analytical techniques in bioanalysis 427\u003c\/p\u003e \u003cp\u003e20.2 Environmental-responsive polymers 428\u003c\/p\u003e \u003cp\u003e20.3 Preparation of a polymer-modified surface for the stationary phase of environmental-responsive chromatography 430\u003c\/p\u003e \u003cp\u003e20.4 Temperature-responsive chromatography for green analytical methods 432\u003c\/p\u003e \u003cp\u003e20.5 Biological analysis by temperature-responsive chromatography 432\u003c\/p\u003e \u003cp\u003e20.5.1 Analysis of propofol in plasma using water as a mobile phase 434\u003c\/p\u003e \u003cp\u003e20.5.2 Contraceptive drugs analysis using temperature gradient chromatography 435\u003c\/p\u003e \u003cp\u003e20.6 Affinity chromatography for green bioseparation 436\u003c\/p\u003e \u003cp\u003e20.7 Separation of biologically active molecules by the green chromatographic method 438\u003c\/p\u003e \u003cp\u003e20.8 Protein separation by an aqueous chromatographic system 441\u003c\/p\u003e \u003cp\u003e20.9 Ice chromatography 442\u003c\/p\u003e \u003cp\u003e20.10 High-temperature liquid chromatography 443\u003c\/p\u003e \u003cp\u003e20.11 Ionic liquids 443\u003c\/p\u003e \u003cp\u003e20.12 The future in green bioanalysis 444\u003c\/p\u003e \u003cp\u003eReferences 444\u003c\/p\u003e \u003cp\u003e\u003cb\u003e21 Infrared Spectroscopy in Biodiagnostics: A Green Analytical Approach 449\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMohammadreza Khanmohammadi and Amir Bagheri Garmarudi\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e21.1 Infrared spectroscopy capabilities 449\u003c\/p\u003e \u003cp\u003e21.2 Infrared spectroscopy of bio-active chemicals in a bio-system 451\u003c\/p\u003e \u003cp\u003e21.3 Medical analysis of body fluids by infrared spectroscopy 453\u003c\/p\u003e \u003cp\u003e21.3.1 Blood and its extracts 455\u003c\/p\u003e \u003cp\u003e21.3.2 Urine 457\u003c\/p\u003e \u003cp\u003e21.3.3 Other body fluids 457\u003c\/p\u003e \u003cp\u003e21.4 Diagnosis in tissue samples via IR spectroscopic analysis 457\u003c\/p\u003e \u003cp\u003e21.4.1 Main spectral characteristics 459\u003c\/p\u003e \u003cp\u003e21.4.2 The role of data processing 460\u003c\/p\u003e \u003cp\u003e21.4.3 Cancer diagnosis by FTIR spectrometry 465\u003c\/p\u003e \u003cp\u003e21.5 New trends in infrared spectroscopy assisted biodiagnostics 468\u003c\/p\u003e \u003cp\u003eReferences 470\u003c\/p\u003e \u003cp\u003e\u003cb\u003e22 Environmental Analysis 475\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eRicardo Erthal Santelli, Marcos Almeida Bezerra, Julio Carlos Afonso, Maria de Fátima Batista de Carvalho, Eliane Padua Oliveira and Aline Soares Freire\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e22.1 Pollution and its control 475\u003c\/p\u003e \u003cp\u003e22.2 Steps of an environmental analysis 476\u003c\/p\u003e \u003cp\u003e22.2.1 Sample collection 476\u003c\/p\u003e \u003cp\u003e22.2.2 Sample preparation 476\u003c\/p\u003e \u003cp\u003e22.2.3 Analysis 479\u003c\/p\u003e \u003cp\u003e22.3 Green environmental analysis for water, wastewater and effluent 480\u003c\/p\u003e \u003cp\u003e22.3.1 Major mineral constituents 480\u003c\/p\u003e \u003cp\u003e22.3.2 Trace metal ions 481\u003c\/p\u003e \u003cp\u003e22.3.3 Organic pollutants 483\u003c\/p\u003e \u003cp\u003e22.4 Green environmental analysis applied for solid samples 485\u003c\/p\u003e \u003cp\u003e22.4.1 Soil 485\u003c\/p\u003e \u003cp\u003e22.4.2 Sediments 488\u003c\/p\u003e \u003cp\u003e22.4.3 Wastes 492\u003c\/p\u003e \u003cp\u003e22.5 Green environmental analysis applied for atmospheric samples 496\u003c\/p\u003e \u003cp\u003e22.5.1 Gases 496\u003c\/p\u003e \u003cp\u003e22.5.2 Particulates 497\u003c\/p\u003e \u003cp\u003eReferences 497\u003c\/p\u003e \u003cp\u003e\u003cb\u003e23 Green Industrial Analysis 505\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eSergio Armenta and Miguel de la Guardia\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e23.1 Greening industrial practices for safety and cost reasons 505\u003c\/p\u003e \u003cp\u003e23.2 The quality control of raw materials and end products 506\u003c\/p\u003e \u003cp\u003e23.3 Process control 510\u003c\/p\u003e \u003cp\u003e23.4 Effluent control 511\u003c\/p\u003e \u003cp\u003e23.5 Working atmosphere control 514\u003c\/p\u003e \u003cp\u003e23.6 The future starts now 515\u003c\/p\u003e \u003cp\u003eReferences 515\u003c\/p\u003e \u003cp\u003e\u003ci\u003eIndex\u003c\/i\u003e 519\u003c\/p\u003e\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003eSubject Areas: Chemistry [\u003ca title=\"See our other books on Chemistry\" href=\"https:\/\/freshlyprintedbooks.co.uk\/search?q=%22Chemistry%20%5BPN%5D%22\"\u003ePN\u003c\/a\u003e]\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\r\n\u003c\/font\u003e","brand":"Wiley","offers":[{"title":"Brand New","offer_id":52278162587928,"sku":"9780470972014","price":102.89,"currency_code":"GBP","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0730\/2037\/5320\/files\/9780470972014.jpg?v=1781458726","url":"https:\/\/freshlyprintedbooks.co.uk\/products\/handbook-of-green-analytical-chemistry-hardback-9780470972014","provider":"Freshly Printed Books","version":"1.0","type":"link"}