{"product_id":"essential-methods-of-instrumental-analysis-hardback-9781394226719","title":"Essential Methods of Instrumental Analysis (Hardback) 9781394226719","description":"\u003cfont face=\"Georgia\"\u003e\r\n\u003cp\u003e\u003cfont size=\"6\"\u003eEssential Methods of Instrumental Analysis\u003c\/font\u003e\u003cbr\u003e\r\n\r\n\r\n\r\n\r\n\r\n\u003c\/p\u003e\n\u003cp\u003e\u003cfont size=\"4\"\u003eFrank M. Dunnivant (Author), Jake W. Ginsbach (Author)\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e9781394226719, Wiley\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003eHardback, published 30 July 2024\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e384 pages\u003cbr\u003e25.4 x 18.3 x 2.3 cm, 0.975 kg\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\r\n\r\n\r\n\r\n\u003cp align=\"justify\"\u003e\u003cstrong\u003e\u003cfont size=\"3\"\u003e\u003cp\u003e\u003cb\u003eIntuitively organized textbook aligned to common analytical instrumentation courses for undergraduate students\u003c\/b\u003e \u003c\/p\u003e\n\u003cp\u003eThrough an analytical approach, \u003ci\u003eEssential Methods of Instrumental Analysis \u003c\/i\u003eprovides an expansive overview of common instruments and methods and their applications for undergraduate students, integrating experimental protocols with real result examples to deliver a well-rounded understanding of the inner workings of the instruments and enabling students to evaluate the success of their experiments and create scientific figures. \u003c\/p\u003e\n\u003cp\u003eIn addition to detailed coverage of specific instruments, the book discusses analytical laboratory practices, instrument maintenance, statistics, and real-world lab experiments with previous student results. Each analytical method section includes extensive sample preparation information, rather than a simple stand-alone chapter offering generic discussions not connected to specific methods. \u003c\/p\u003e\n\u003cp\u003eThis book conveniently organizes content by analyte class (inorganic and organic) in a way that is intuitive to a student and aligned with relevant courses. Ancillaries including .mp4 videos, instructor PowerPoint slides, and animations are included on a companion website. \u003c\/p\u003e\n\u003cp\u003eWritten by an experienced professor and tested and refined over years in his courses since 2008, \u003ci\u003eEssential Methods of Instrumental Analysis\u003c\/i\u003e includes information on sample topics such as: \u003c\/p\u003e\n\u003cul\u003e\n\u003cli\u003eProper laboratory protocols for analytical instrumentation, covering chemical reagents, glassware, calibration techniques, and figures of merit\u003c\/li\u003e\n\u003cli\u003eOptical physics, covering the interaction of electromagnetic radiation with instrument components and sample molecules, relaxation processes, reflection, diffraction, dispersion, and refraction\u003c\/li\u003e\n\u003cli\u003eFlame atomic absorption and flame emission spectrometry, covering optical radiation sources, mirrors, choppers, burner heads, and doppler broadening\u003c\/li\u003e\n\u003cli\u003eGas and liquid chromatography, covering gaseous, liquid, soil-sediment, and biological samples, analyte recovery, chromatography theory, injectors, columns and ovens, common detectors, and mass spectrometers\u003c\/li\u003e\n\u003c\/ul\u003e \u003cp\u003eFocusing on contrasts and comparisons across multiple types of instruments in a way distinct from similar texts, \u003ci\u003eEssential Methods of Instrumental Analysis \u003c\/i\u003eis an essential textbook for students in advanced undergraduate courses in related programs of study.\u003c\/p\u003e\u003c\/font\u003e\u003c\/strong\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003e\u003cp\u003eAbout the Authors xv\u003c\/p\u003e \u003cp\u003ePreface xix\u003c\/p\u003e \u003cp\u003eAbout the Companion Website\u003ci\u003e xxi\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Proper Laboratory Protocols for Analytical Instrumentation 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e1.1 Laboratory Preliminaries 1\u003c\/p\u003e \u003cp\u003e1.2 Standard Practices 11\u003c\/p\u003e \u003cp\u003e1.3 Questions 13\u003c\/p\u003e \u003cp\u003e1.4 Problems 14\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Statistical Analysis 17\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e2.1 Introduction 17\u003c\/p\u003e \u003cp\u003e2.2 Linear Least-squares Analysis 18\u003c\/p\u003e \u003cp\u003e2.3 Student’s t-test Equations 20\u003c\/p\u003e \u003cp\u003e2.4 Assignments 24\u003c\/p\u003e \u003cp\u003eFurther Reading 24\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 A Review of Optical Physics 25\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e3.1 Introduction 25\u003c\/p\u003e \u003cp\u003e3.2 Interaction of Electromagnetic Radiation with Sample Molecules 26\u003c\/p\u003e \u003cp\u003e3.3 Interaction of Electromagnetic Radiation with Surfaces 32\u003c\/p\u003e \u003cp\u003e3.4 Detectors in UV–visible Spectrometry 41\u003c\/p\u003e \u003cp\u003e3.5 Summary 48\u003c\/p\u003e \u003cp\u003eReference 49\u003c\/p\u003e \u003cp\u003e3.6 Questions 49\u003c\/p\u003e \u003cp\u003eSupporting Information 51\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Analytical Molecular Spectrometry 53\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e4.1 Introduction 53\u003c\/p\u003e \u003cp\u003e4.2 Basic UV–Vis Spectrometer 53\u003c\/p\u003e \u003cp\u003e4.3 From Simple to Complex UV–Visible Spectrometers 54\u003c\/p\u003e \u003cp\u003e4.4 Fluorescence and Phosphorescence Instruments 55\u003c\/p\u003e \u003cp\u003e4.5 Instrument Maintenance 57\u003c\/p\u003e \u003cp\u003e4.6 Summary 57\u003c\/p\u003e \u003cp\u003e4.7 Case Study: Quantitation of Riboflavin by UV–Vis and Fluorescence Spectrometry by Nate Boland 60\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Flame Atomic Absorption and Flame Emission Spectrometry 61\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e5.1 Introduction and History of Atomic Absorption Spectrometry (AAS) 61\u003c\/p\u003e \u003cp\u003e5.2 Components of a Flame Atomic Absorption\/Emission Spectrometer System 61\u003c\/p\u003e \u003cp\u003e5.3 Specialized Sample Introduction Techniques and Analysis 73\u003c\/p\u003e \u003cp\u003e5.4 General Operation of FAAS and FAES Instruments 76\u003c\/p\u003e \u003cp\u003e5.5 Maintenance 76\u003c\/p\u003e \u003cp\u003e5.6 Summary 76\u003c\/p\u003e \u003cp\u003e5.7 Questions 77\u003c\/p\u003e \u003cp\u003eSupporting Information 78\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Inductively Coupled Plasma 79\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e6.1 Introduction and History 79\u003c\/p\u003e \u003cp\u003e6.2 Atomic Emission Spectrometry Theory 79\u003c\/p\u003e \u003cp\u003e6.3 Components of an Inductively Coupled Plasma: Atomic Emission Spectrometry System (ICP–AES) 80\u003c\/p\u003e \u003cp\u003e6.4 Interferences 90\u003c\/p\u003e \u003cp\u003e6.5 Maintenance 90\u003c\/p\u003e \u003cp\u003e6.6 Case Study: Quantitation of Heavy Metals in Consumer Products by Dan Burgard 90\u003c\/p\u003e \u003cp\u003e6.7 Summary 91\u003c\/p\u003e \u003cp\u003e6.8 Questions 92\u003c\/p\u003e \u003cp\u003eSupporting Information 92\u003c\/p\u003e \u003cp\u003eReferences 93\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Inductively Coupled Plasma–Mass Spectrometry 95\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e7.1 Introduction and History 95\u003c\/p\u003e \u003cp\u003e7.2 Components of a Mass Spectrometer 95\u003c\/p\u003e \u003cp\u003e7.3 Summary 112\u003c\/p\u003e \u003cp\u003e7.4 Questions 113\u003c\/p\u003e \u003cp\u003eSupporting Information 115\u003c\/p\u003e \u003cp\u003eReference 115\u003c\/p\u003e \u003cp\u003eFurther Reading 115\u003c\/p\u003e \u003cp\u003e\u003cb\u003e8 Contrasts and Comparisons of Instrumentation 117\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e8.1 Introduction 117\u003c\/p\u003e \u003cp\u003e8.2 Figures of Merit 117\u003c\/p\u003e \u003cp\u003e8.3 Questions 120\u003c\/p\u003e \u003cp\u003e\u003cb\u003e9 Chromatography Introduction, Chromatography Theory, and Instrument Calibration 121\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e9.1 Introduction 121\u003c\/p\u003e \u003cp\u003e9.2 Chromatographic Theory 122\u003c\/p\u003e \u003cp\u003e9.3 Case Study 129\u003c\/p\u003e \u003cp\u003e9.4 Optimization of Chromatographic Conditions 131\u003c\/p\u003e \u003cp\u003e9.5 Calibration of an Instrument\/Detector 133\u003c\/p\u003e \u003cp\u003e9.6 Evolution of Peak Integration 135\u003c\/p\u003e \u003cp\u003eSupporting Information 136\u003c\/p\u003e \u003cp\u003eReferences 136\u003c\/p\u003e \u003cp\u003e\u003cb\u003e10 Gas Chromatography 137\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e10.1 Introduction and History 137\u003c\/p\u003e \u003cp\u003e10.2 Types of Samples and Sample Introduction 137\u003c\/p\u003e \u003cp\u003e10.3 Gas Chromatography 143\u003c\/p\u003e \u003cp\u003e10.4 Advanced GC Systems 152\u003c\/p\u003e \u003cp\u003e10.5 Applications\/Case Studies 152\u003c\/p\u003e \u003cp\u003e10.6 Summary 160\u003c\/p\u003e \u003cp\u003e10.7 Questions 161\u003c\/p\u003e \u003cp\u003eSupporting Information 162\u003c\/p\u003e \u003cp\u003eReference 162\u003c\/p\u003e \u003cp\u003e\u003cb\u003e11 High-performance Liquid Chromatography 163\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e11.1 Introduction and History 163\u003c\/p\u003e \u003cp\u003e11.2 Types of Analytes, Samples, and Sample Introduction 165\u003c\/p\u003e \u003cp\u003e11.3 Liquid Chromatography 166\u003c\/p\u003e \u003cp\u003e11.4 Advanced and Specialty LC Systems 173\u003c\/p\u003e \u003cp\u003e11.5 Applications\/Case Studies 177\u003c\/p\u003e \u003cp\u003e11.6 Summary 180\u003c\/p\u003e \u003cp\u003e11.7 Questions 180\u003c\/p\u003e \u003cp\u003eSupporting Information 182\u003c\/p\u003e \u003cp\u003eReferences 182\u003c\/p\u003e \u003cp\u003e\u003cb\u003e12 Capillary Electrophoresis by Nicole James 185\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e12.1 Introduction 185\u003c\/p\u003e \u003cp\u003e12.2 Electrophoresis and Capillary Electrophoresis 185\u003c\/p\u003e \u003cp\u003e12.3 Samples 190\u003c\/p\u003e \u003cp\u003e12.4 Methods of Operation 192\u003c\/p\u003e \u003cp\u003e12.5 Detectors 195\u003c\/p\u003e \u003cp\u003e12.6 Application\/Case Studies 199\u003c\/p\u003e \u003cp\u003e12.7 Summary 202\u003c\/p\u003e \u003cp\u003eReferences 202\u003c\/p\u003e \u003cp\u003e\u003cb\u003e13 Mass Spectrometry 203\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e13.1 Introduction and History 203\u003c\/p\u003e \u003cp\u003e13.2 Sample Introduction from GC and Analyte Ionization 204\u003c\/p\u003e \u003cp\u003e13.3 Introduction of Samples from HPLC 210\u003c\/p\u003e \u003cp\u003e13.4 Introduction of Samples from a Capillary Electrophoresis System 214\u003c\/p\u003e \u003cp\u003e13.5 Common Mass Filters (Mass Analyzers) 216\u003c\/p\u003e \u003cp\u003e13.6 Ion Detectors 238\u003c\/p\u003e \u003cp\u003e13.7 Three-dimensional Aspects of GC–MS 239\u003c\/p\u003e \u003cp\u003e13.8 Summary 239\u003c\/p\u003e \u003cp\u003e13.9 Questions 240\u003c\/p\u003e \u003cp\u003eSupporting Information 242\u003c\/p\u003e \u003cp\u003eReferences 242\u003c\/p\u003e \u003cp\u003eFurther Reading 242\u003c\/p\u003e \u003cp\u003e\u003cb\u003e14 Fragmentation and Interpretation of Spectra 245\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e14.1 Introduction 245\u003c\/p\u003e \u003cp\u003e14.2 Creation of the Spectra 246\u003c\/p\u003e \u003cp\u003e14.3 Identifying the Molecular Ion Peak 247\u003c\/p\u003e \u003cp\u003e14.4 Use of the Molecular Ion 249\u003c\/p\u003e \u003cp\u003e14.5 Identification of Analytes Using Isotopic Ratios 252\u003c\/p\u003e \u003cp\u003e14.6 Fragmentation 255\u003c\/p\u003e \u003cp\u003e14.7 Rearrangements 257\u003c\/p\u003e \u003cp\u003e14.8 Identification of Compounds 257\u003c\/p\u003e \u003cp\u003e14.9 Fragmentation of Hydrocarbons 258\u003c\/p\u003e \u003cp\u003e14.10 Fragmentation of Alcohols 262\u003c\/p\u003e \u003cp\u003e14.11 Fragmentation of Ketones and Aldehydes 265\u003c\/p\u003e \u003cp\u003e14.12 Fragmentation of Carboxylic Acids 270\u003c\/p\u003e \u003cp\u003e14.13 Fragmentation of Ethers 271\u003c\/p\u003e \u003cp\u003e14.14 Fragmentation of Esters 273\u003c\/p\u003e \u003cp\u003e14.15 Fragmentation of Amines 276\u003c\/p\u003e \u003cp\u003e14.16 Fractionation of Amides 278\u003c\/p\u003e \u003cp\u003e14.17 Fragmentation of Nitriles 279\u003c\/p\u003e \u003cp\u003e14.18 Reviewing General Principles 280\u003c\/p\u003e \u003cp\u003e14.19 Searchable Databases 284\u003c\/p\u003e \u003cp\u003e\u003cb\u003e15 Common Radiochemical Detection Methods in Analytical Chemistry 285\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e15.1 Introduction 285\u003c\/p\u003e \u003cp\u003e15.2 Common Sources of Radiation 285\u003c\/p\u003e \u003cp\u003e15.3 Detection of Alpha, Beta, and Gamma Emission 286\u003c\/p\u003e \u003cp\u003e15.4 Case Studies 290\u003c\/p\u003e \u003cp\u003eReference 290\u003c\/p\u003e \u003cp\u003e\u003cb\u003e16 Instrumental Laboratory Experiments with Results 291\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e16.1 Introduction 291\u003c\/p\u003e \u003cp\u003e16.2 A Typical Glassware Inventory for an Instrumental Methods Course 291\u003c\/p\u003e \u003cp\u003e16.3 Maintaining a Legally Defensible Laboratory Notebook 291\u003c\/p\u003e \u003cp\u003e16.4 Solutions, Weights, and Laboratory Techniques 293\u003c\/p\u003e \u003cp\u003e16.5 Determination of a Surrogate Toxic Metal (Ca) in a Simulated Hazardous Waste Sample by a Variety of Techniques 295\u003c\/p\u003e \u003cp\u003e16.6 Identification of Components in Liquors and Distilled Spirits 306\u003c\/p\u003e \u003cp\u003e16.7 Identification of Fragrances 311\u003c\/p\u003e \u003cp\u003e16.8 GC–MS Analysis of Synthetic and Natural Fragrances by Evan Bowman, Annika Mayo, and Aurora Anderson 316\u003c\/p\u003e \u003cp\u003e16.9 SPME–GC–MS Analysis of Wine Headspace by Bailey Arend 324\u003c\/p\u003e \u003cp\u003e16.10 Quantitative Determination of the Presence of Captan on Organic and Nonorganic Strawberries by Peter Mullin, Eric Ying, Jon Na, Sharon Ndayambaje, and Soren Sandeno 330\u003c\/p\u003e \u003cp\u003e16.11 Determination of Nicotine in Human Urine Using HPLC–MS by Ashley Nguyen, Lea Molacek, Maxwell Brown 333\u003c\/p\u003e \u003cp\u003e16.12 Analysis of Caffeine in Urine Samples Using GC–FID by Elsa Nader, Ralph Huang, Aaron Lieberman, Jane Duncan, and Matt Sousa 336\u003c\/p\u003e \u003cp\u003e16.13 Caffeine in the Walla Walla (WA) Wastewater Effluent by MacKenzie Cummings, Mia Groff, Roya Nasseri, Noah Willis, and Clara Wheeler 338\u003c\/p\u003e \u003cp\u003e16.14 Gasoline Analysis by GC–FID and GC–MS by Theodore Pierce and Austin Shaff 340\u003c\/p\u003e \u003cp\u003e16.15 GC–MS as an Effective Instrument for Detecting Cocaine on US Currency by Jessica Boyers and Kacey Godwin 343\u003c\/p\u003e \u003cp\u003e16.16 Analytical Quantification of CBD-A Content in Cannabis sativa (Hemp) Using GC–FID and GC–MS by Lauren Yumibe, Sam Weiss, Maddie Bowers, Tori Li, Asher Bachtold, and Brandon Neifert 347\u003c\/p\u003e \u003cp\u003e16.17 Results and Discussion 349\u003c\/p\u003e \u003cp\u003e16.18 Conclusions 350\u003c\/p\u003e \u003cp\u003eReferences 351\u003c\/p\u003e \u003cp\u003eFurther Reading 354\u003c\/p\u003e \u003cp\u003eIndex 357\u003c\/p\u003e\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\u003cp\u003e\u003cfont size=\"3\"\u003eSubject Areas: Chemistry [\u003ca title=\"See our other books on Chemistry\" href=\"https:\/\/freshlyprintedbooks.co.uk\/search?q=%22Chemistry%20%5BPN%5D%22\"\u003ePN\u003c\/a\u003e]\u003c\/font\u003e\u003c\/p\u003e\r\n\r\n\r\n\u003c\/font\u003e","brand":"Wiley","offers":[{"title":"Brand New","offer_id":52433219354904,"sku":"9781394226719","price":77.39,"currency_code":"GBP","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0730\/2037\/5320\/files\/9781394226719.jpg?v=1784852088","url":"https:\/\/freshlyprintedbooks.co.uk\/products\/essential-methods-of-instrumental-analysis-hardback-9781394226719","provider":"Freshly Printed Books","version":"1.0","type":"link"}